Other grades of this product :
| DIGITOXIGENIN Basic information |
| Product Name: | DIGITOXIGENIN | | Synonyms: | 5BETA,20[22]-CARDENOLIDE-3BETA,14-DIOL;3BETA,14-DIHYDROXY-5BETA,20[22]-CARDENOLIDE;20(22),5BETA-CARDENOLID-3BETA,14BETA-DIOL;3,14,21-TRIHYDROXY-20(22)-NORCHOLENIC ACID LACTONE;cerberigenin;delta-sup(20:22)-3,14,21-trihydroxynorcholenicacidlactone;digitoxigenine;echujetin | | CAS: | 143-62-4 | | MF: | C23H34O4 | | MW: | 374.51 | | EINECS: | 205-603-4 | | Product Categories: | Biochemistry;Steroids;Steroids (Others);ATPase | | Mol File: | 143-62-4.mol |
| DIGITOXIGENIN Chemical Properties |
| Melting point | 253-255 °C (dec.)(lit.) | | alpha | D17 +19.1° (c = 1.36 in methanol) | | Boiling point | 423.5°C (rough estimate) | | density | 1.0284 (rough estimate) | | refractive index | 1.4433 (estimate) | | pka | 14.93±0.70(Predicted) | | form | powder to crystal | | color | White to Almost white | | Water Solubility | 11.24mg/L(30 ºC) | | Merck | 14,3162 | | BRN | 95448 | | CAS DataBase Reference | 143-62-4(CAS DataBase Reference) |
| Hazard Codes | T | | Risk Statements | 25 | | Safety Statements | 45 | | RIDADR | UN 3462 6.1/PG 2 | | WGK Germany | 3 | | RTECS | FH4975000 | | HazardClass | 6.1(a) | | PackingGroup | II |
| DIGITOXIGENIN Usage And Synthesis |
| Uses | Cardiotonic;Na+ K+ ATPase inhibitor | | Purification Methods | Dissolve digitoxigenin in EtOAc, wash it with H2O, dry it (Na2SO4), evaporate and recrystallise it from 40% aqueous EtOH or aqueous MeOH then EtOAc/Et2O. The UV has max at 218nm ( 14,500 M-1cm-1). The 3-acetate crystallises from Me2CO/Et2O with m 222-227o, [] D 20 +21o (c 1, CHCl3). [Wyss et al. Helv Chim Acta 43 644 1960, Cruz et al. J Org Chem 4 2 3580 1977, Beilstein 18 IV 1468.] |
| DIGITOXIGENIN Preparation Products And Raw materials |
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