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| 1-Iodo-3-methylbutane Basic information |
| 1-Iodo-3-methylbutane Chemical Properties |
| Melting point | -85.6°C (estimate) | | Boiling point | 149 °C(lit.) | | density | 1.497 g/mL at 25 °C(lit.) | | refractive index | n20/D 1.492(lit.) | | Fp | 115 °F | | storage temp. | Flammables area | | form | clear liquid | | color | Colorless to Light yellow to Light orange | | Water Solubility | Insoluble in water. Soluble in most common organic solvents. | | Sensitive | Light Sensitive | | Merck | 14,5120 | | BRN | 1730990 | | CAS DataBase Reference | 541-28-6(CAS DataBase Reference) | | NIST Chemistry Reference | Butane, 1-iodo-3-methyl-(541-28-6) | | EPA Substance Registry System | Butane, 1-iodo-3-methyl- (541-28-6) |
| Hazard Codes | Xn,Xi | | Risk Statements | 10-22 | | Safety Statements | 16 | | RIDADR | UN 1993 3/PG 3 | | WGK Germany | 3 | | RTECS | EK4412000 | | F | 1-8-9 | | Hazard Note | Irritant | | TSCA | Yes | | HazardClass | 3 | | PackingGroup | III | | HS Code | 29033080 |
| 1-Iodo-3-methylbutane Usage And Synthesis |
| Chemical Properties | clear slightly yellow to pink liquid | | Uses | 1-Iodo-3-methylbutane can be used for organic synthesis or used as solvents. | | Preparation | Synthesis of 1-Iodo-3-methylbutane: Bromo-3-methylbutane (30.2 g, 0.20 mol) was added dropwise to a mixture of NaI (44.97g, 0.30 mol) and acetone (500 mL). The mixture was refluxed overnight. The mixture was filtrated and the filter cake was washed with (2 x 50 mL) acetone. The acetone was evaporated under reduced pressure. 1-Iodo-3-methylbutane was distilled under vacuum to give 13.8g (35 %) (b.p. 25 - 35°C, 15 mmHg). |
| 1-Iodo-3-methylbutane Preparation Products And Raw materials |
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