| TRIMETHYLSILYLBENZENESULFONATE Basic information |
| Product Name: | TRIMETHYLSILYLBENZENESULFONATE |
| Synonyms: | (PHENYLSULFONYLMETHYL)TRIMETHYLSILANE;PHENYL TRIMETHYLSILYLMETHYL SULFONE;TRIMETHYLSILYLBENZENESULPHONATE;TRIMETHYLSILYLBENZENESULFONATE;Trimethylsilybenzenesulfonate;(Phenylsulfonylmethyl)trimethylsilane, (Trimethylsilyl)methyl phenyl sulfone;PhenylTrimethylsilylmethylSulfone>benzenesulfonylmethyl(trimethyl)silane |
| CAS: | 17872-92-3 |
| MF: | C10H16O2SSi |
| MW: | 228.38 |
| EINECS: | 679-678-0 |
| Product Categories: | Sulfur Compounds (for Synthesis);Synthetic Organic Chemistry;Si (Classes of Silicon Compounds);Si-(C)4 Compounds;Silicon Compounds (for Synthesis) |
| Mol File: | 17872-92-3.mol |
| TRIMETHYLSILYLBENZENESULFONATE Chemical Properties |
| Melting point | 28-32 °C |
| Boiling point | 154-156 °C(lit.) |
| density | 1.138 g/mL at 25 °C(lit.) |
| refractive index | n |
| Fp | 48 °F |
| storage temp. | 2-8°C |
| form | powder to lump to clear liquid |
| color | White or Colorless to Almost white or Almost colorless |
| Safety Information |
| Hazard Codes | F,Xi |
| Risk Statements | 36/37/38 |
| Safety Statements | 26-36 |
| RIDADR | UN 3272 3/PG 2 |
| WGK Germany | 3 |
| F | 10-21 |
| MSDS Information |
| Provider | Language |
|---|---|
| SigmaAldrich | English |
| TRIMETHYLSILYLBENZENESULFONATE Usage And Synthesis |
| Purification Methods | Fractionate it at high vacuum and recrystallise it from pentane at -80o. If too impure (cf IR), dissolve it in CH2Cl2 (ca 800mL for 100g), wash this with 2M aqueous NaOH (2 x 200mL), brine, dry, evaporate and distil it. [Craig et al. J Chem Soc, Perkin Trans 1 1949 1985, IR and NMR: Cooper J Am Chem Soc 76 3713 1954.] |
| TRIMETHYLSILYLBENZENESULFONATE Preparation Products And Raw materials |
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