CYCLODECANONE

CYCLODECANONE
  • CAS No.:1502-06-3
Other grades of this product :
CYCLODECANONE Basic information
Product Name:CYCLODECANONE
Synonyms:CYCLODECANONE CRYSTALLINE;Ketocyclodecane;Cyclodecanone,97%;NSC 90293;CYCLODECAN-1-ONE;CYCLODECANONE;Cyclodecanone 97%;N-(6-amino-1-methyl-2,4-dioxo-5-pyrimidinyl)formamide
CAS:1502-06-3
MF:C10H18O
MW:154.25
EINECS:216-119-8
Product Categories:C10;Carbonyl Compounds;Ketones
Mol File:1502-06-3.mol
CYCLODECANONE Chemical Properties
Melting point 21-24 °C (lit.)
Boiling point 106-107 °C/12 mmHg (lit.)
density 0.958 g/mL at 25 °C (lit.)
refractive index n20/D 1.482(lit.)
Fp 180 °F
storage temp. 2-8°C
solubility Chloroform (Slightly), Methanol (Slightly)
form Colourless Oil to Semi-Solid
BRN 1617127
Safety Information
Hazard Codes Xi
Risk Statements 36
Safety Statements 26
WGK Germany 3
9-23
HS Code 29142990
MSDS Information
ProviderLanguage
SigmaAldrich English
CYCLODECANONE Usage And Synthesis
Chemical PropertiesWhite solid or colorless liquid
Synthesis Reference(s)Journal of the American Chemical Society, 86, p. 3068, 1964 DOI: 10.1021/ja01069a019Organic Syntheses, Coll. Vol. 4, p. 218, 1963Synthetic Communications, 9, p. 437, 1979 DOI: 10.1080/00397917908064174
Purification MethodsPurify the ketone via the semicarbazone (m 205-207o, from EtOH) and distil it through an efficient column. It sublimes in a vacuum. The oxime has m 80o, from MeOH or by sublimation in a high vacuum. [Cope et al. Org Synth Coll Vol IV 218 1963, Prelog et al. Helv Chim Acta 30 1746 1947, Ruzicka et al. Helv Chim Acta 11 675 1930, Beilstein 7 III 134, 7 IV 76.]
CYCLODECANONE Preparation Products And Raw materials
Preparation ProductsN-cyclodecylmethylamine

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