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| METHYL 1-BROMOCYCLOHEXANECARBOXYLATE Basic information |
| Product Name: | METHYL 1-BROMOCYCLOHEXANECARBOXYLATE | | Synonyms: | METHYL 1-BROMOCYCLOHEXANECARBOXYLATE, 97 %;LABOTEST-BB LT00160081;METHYL 1-BROMOCYCLOHEXANECARBOXYLATE;Methyl 1-broMocyclohexanecarboxylate 97%;1-Bromocyclohexanecarboxylic acid methyl ester;Cyclohexanecarboxylic acid, 1-bromo-, methyl ester;methyl 1-bromocyclohexane-1-carboxylate | | CAS: | 3196-23-4 | | MF: | C8H13BrO2 | | MW: | 221.09 | | EINECS: | | Product Categories: | C8 to C9;Carbonyl Compounds;Esters | | Mol File: | 3196-23-4.mol |
| METHYL 1-BROMOCYCLOHEXANECARBOXYLATE Chemical Properties |
| Boiling point | 115-116 °C/19 mmHg (lit.) | | density | 1.39 g/mL at 25 °C (lit.) | | refractive index | n20/D 1.493(lit.) | | Fp | 222 °F | | storage temp. | 2-8°C |
| METHYL 1-BROMOCYCLOHEXANECARBOXYLATE Usage And Synthesis |
| Uses | Methyl 1-bromocyclohexanecarboxylate may be used in the improved method of preparation of methyl 3-oxo-1-cyclohexene-1-carboxylate. It may be used in the Reformatsky synthesis of 16-aryl-15-oxadispiro[5.1.5.3]hexadecane-7,14-diones. | | General Description | Methyl 1-bromocyclohexanecarboxylate reacts with zinc and substituted chalcones to yield the corresponding spiro-3,4-dihydropyran-2-one derivatives, 3-aryl-5-aryl-2-oxaspiro[5.5]undec-3-en-1-ones. Reformatsky reaction of methyl 1-bromocyclohexanecarboxylate with 2-aryl-2-oxoacetaldehyde is reported. Methyl 1-bromocyclohexanecarboxylate reacts with zinc and amides or methylamides of 3-aryl-2-cyanopropenoic acids to yield 5-aryl-1,3-dioxo-2-azaspiro[5.5]undecane-4-carbonitriles or 5-aryl-2-methyl-1,3-dioxo-2-azaspiro[5.5]undecane-4-carbonitriles. |
| METHYL 1-BROMOCYCLOHEXANECARBOXYLATE Preparation Products And Raw materials |
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