BIS(PHENYLTHIO)METHANE

CAS No.：3561-67-9

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BIS(PHENYLTHIO)METHANE Basic information

Product Name:	BIS(PHENYLTHIO)METHANE
Synonyms:	BIS(PHENYLTHIO)METHANE;1-(methylthio)-2-(phenylthio)benzene;1,1'-(Methanediyldisulfanediyl)dibenzene;1-([(PHENYLTHIO)METHYL]THIO)BENZENE;DIPHENYLTHIOMETHANE;FORMALDEHYDE DIPHENYL MERCAPTAL;1,1'-(METHYLENEBIS(THIO))BISBENZENE;[methylenebis(thio)]bisbenzene
CAS:	3561-67-9
MF:	C13H12S2
MW:	232.36
EINECS:	222-624-4
Product Categories:	Sulfur Compounds (for Synthesis);Synthetic Organic Chemistry
Mol File:	3561-67-9.mol

BIS(PHENYLTHIO)METHANE Chemical Properties

Melting point	34-37 °C(lit.)
Boiling point	194 °C8 mm Hg(lit.)
density	1.2633 (rough estimate)
refractive index	1.6210 (estimate)
Fp	>230 °F
storage temp.	Sealed in dry,Room Temperature
form	powder to crystal
color	White to Light yellow
Water Solubility	Insoluble in water.
BRN	1874146
CAS DataBase Reference	3561-67-9(CAS DataBase Reference)

Safety Information

Hazard Codes	Xi
Risk Statements	36/37/38
Safety Statements	26-36
RIDADR	UN 3335
WGK Germany	3
F	13
HazardClass	STENCH
HS Code	29309090

MSDS Information

Provider	Language
ACROS	English
SigmaAldrich	English
ALFA	English

BIS(PHENYLTHIO)METHANE Usage And Synthesis

Chemical Properties	light yellow crystalline powder
Uses	Bis(phenylthio)methane (PhSCH₂SPh) may be used in the synthesis of the following: dihydroxy thioethers [Cu₄I₄{μ-PhS₂CH₂SPh}₂]_n [(η⁵-C₅Me₅)MCl₂(η¹-(PhS)₂CH₂)] (M=Rh, Ir ; C₅Me₅= pentamethylcyclopentadienyl) 6-deoxy-1,2:3,4-di-O-isopropylidene-α-D-galactoheptodialdo-1,5-pyranose diphenyl dithioacetal
Synthesis Reference(s)	Synthetic Communications, 19, p. 31, 1989 DOI: 10.1080/00397918908050949Synthesis, p. 447, 1975 DOI: 10.1055/s-1975-23797
General Description	Bis(phenylthio)methane (PhSCH₂SPh) is a dithioether ligand. It forms coordination complex with silver(I) salts. It participates in the synthesis of (-)-rasfonin.

BIS(PHENYLTHIO)METHANE Preparation Products And Raw materials

Raw materials	Thiophenol-->Diiodomethane-->SODIUM THIOPHENOXIDE
Preparation Products	7-TRIDECANOL-->Biphenyl-4,4'-dithiol

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