2-(3-METHOXYPHENYL)CYCLOHEXANONE

CAS No.：15547-89-4

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2-(3-METHOXYPHENYL)CYCLOHEXANONE Basic information

Product Name:	2-(3-METHOXYPHENYL)CYCLOHEXANONE
Synonyms:	2-(3-METHOXYPHENYL)CYCLOHEXANONE;2-(3-METHOXYPHENYL)CYCLOHEXANONE, TECH., 90%;2-(3-Methoxyphenyl)cyclohexanone, tech.,90%;2-(3-Methoxyphenyl)cyclohexanone,90%,tech.;2-(3-Methoxyphenyl)cyclohexanone technical grade, 90%;2-(3-METHOXYPHENYL)CYCLOHEXANON;2-(3-methoxyphenyl)cyclohexan-1-one;(2S)-2-(3-methoxyphenyl)-1-cyclohexanone
CAS:	15547-89-4
MF:	C13H16O2
MW:	204.26
EINECS:	239-602-5
Product Categories:	C13 to C14;Carbonyl Compounds;Ketones
Mol File:	15547-89-4.mol

2-(3-METHOXYPHENYL)CYCLOHEXANONE Chemical Properties

Boiling point	140-142°C 0,2mm
density	1.1 g/mL at 25 °C (lit.)
refractive index	n20/D 1.546(lit.)
Fp	>230 °F
CAS DataBase Reference	15547-89-4(CAS DataBase Reference)
EPA Substance Registry System	2-(3-Methoxyphenyl)cyclohexanone (15547-89-4)

Safety Information

Safety Statements	24/25
WGK Germany	3
HS Code	29145000

MSDS Information

Provider	Language
SigmaAldrich	English
ACROS	English
ALFA	English

2-(3-METHOXYPHENYL)CYCLOHEXANONE Usage And Synthesis

Chemical Properties	clear colorless liquid
Uses	2-(3-Methoxyphenyl)cyclohexanone may be used as starting reagent for the synthesis of octahydrophenanthrene, an important intermediate in the synthesis of morphinans. It may be used in the synthesis of 2-methyl-5-phenyl morphan.
Synthesis Reference(s)	The Journal of Organic Chemistry, 20, p. 1197, 1955 DOI: 10.1021/jo01126a008
General Description	2-(3-Methoxyphenyl)cyclohexanone is an aromatic ketone. It is a clear, colorless liquid. 2-(3-Methoxyphenyl)cyclohexanone is reported to participate in the synthesis of 9-azamorphinan.

2-(3-METHOXYPHENYL)CYCLOHEXANONE Preparation Products And Raw materials

Raw materials

Lithium, (3-methoxyphenyl)--->3-METHOXYPHENYLMAGNESIUM BROMIDE-->2-Chlorocyclohexanone-->1-NITRO-1-CYCLOHEXENE-->2-Chloroanisole-->1-Cyclohexenyloxytrimethylsilane-->3-Iodoanisole-->2,2,6,6-Tetramethylpiperidine-->Cyclohexene oxide-->3-Bromoanisole-->Cyclohexanone

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