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| 3'-Methylacetanilide Basic information |
| 3'-Methylacetanilide Chemical Properties |
| Melting point | 65-67 °C (lit.) | | Boiling point | 303 °C (lit.) | | density | 1.1410 | | vapor pressure | 16 mm Hg ( 163 °C) | | refractive index | 1.5279 (estimate) | | storage temp. | Inert atmosphere,Room Temperature | | solubility | alcohol: freely soluble(lit.) | | pka | 15.12±0.70(Predicted) | | form | powder to crystal | | color | White to Light gray to Light yellow | | Merck | 14,74 | | Stability: | Stable. Incompatible with strong oxidizing agents. | | CAS DataBase Reference | 537-92-8(CAS DataBase Reference) | | NIST Chemistry Reference | N-(3-Tolyl)acetic acid amide(537-92-8) | | EPA Substance Registry System | m-Acetotoluidide (537-92-8) |
| Hazard Codes | Xn,Xi | | Risk Statements | 22-36/37/38 | | Safety Statements | 26-36 | | WGK Germany | 3 | | RTECS | AN2875000 | | HS Code | 29242998 | | Toxicity | LD50 orl-mus: 1450 mg/kg TXAPA9 19,20,71 |
| 3'-Methylacetanilide Usage And Synthesis |
| Chemical Properties | white crystalline solid | | General Description | White solid. | | Air & Water Reactions | Water insoluble. | | Reactivity Profile | 3'-Methylacetanilide is an amide. Flammable gases are formed by the reaction of organic amides with strong reducing agents. Amides are very weak bases (weaker than water). Imides are less basic yet and in fact react with strong bases to form salts. That is, they can react as acids. Mixing amides with dehydrating agents such as P2O5 or SOCl2 generates the corresponding nitrile. The combustion of these compounds generates mixed oxides of nitrogen (NOx). | | Health Hazard | ACUTE/CHRONIC HAZARDS: When heated to decomposition 3'-Methylacetanilide emits toxic fumes of nitrogen oxides. | | Fire Hazard | Flash point data for 3'-Methylacetanilide are not available; however, 3'-Methylacetanilide is probably combustible. | | Safety Profile | Moderately toxic by ingestion. Seealso p-ACETOTOLUIDIDE. When heated todecomposition it emits toxic fumes of NOx. | | Purification Methods | Crystallise the toluidide from H2O, EtOH, aqueous EtOH or Et2O/pet ether (m 66o). UV: max 245nm (EtOH). [Beilstein 12 H 860, 12 I 400, 12 II 468, 12 III 1962, 12 IV 1823.] |
| 3'-Methylacetanilide Preparation Products And Raw materials |
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