Other grades of this product :
| 2-Phenoxyethylbromide Basic information |
| 2-Phenoxyethylbromide Chemical Properties |
| Melting point | 31-34 °C(lit.) | | Boiling point | 144 °C40 mm Hg(lit.) | | density | 1.45 | | refractive index | 1.555-1.557 | | Fp | 150 °F | | storage temp. | Keep in dark place,Sealed in dry,Room Temperature | | solubility | Solubility in methanol is almost transparent. Soluble in chloroform and ethyl acetate. | | form | Liquid After Melting | | color | Clear colorless | | Water Solubility | Insoluble in water. | | BRN | 508290 | | CAS DataBase Reference | 589-10-6(CAS DataBase Reference) | | NIST Chemistry Reference | Benzene, (2-bromoethoxy)-(589-10-6) | | EPA Substance Registry System | Benzene, (2-bromoethoxy)- (589-10-6) |
| Hazard Codes | Xi,Xn | | Risk Statements | 36/37/38-22 | | Safety Statements | 23-24/25-26 | | RIDADR | 1325 | | WGK Germany | 3 | | Hazard Note | Irritant | | TSCA | Yes | | HazardClass | 4.1 | | PackingGroup | II | | HS Code | 29093038 |
| 2-Phenoxyethylbromide Usage And Synthesis |
| Chemical Properties | White Solid | | Uses | 2-Phenoxyethyl bromide is used in the synthesis and antihypertensive activity of 4'-substituted spiro[4H-3,1-benzoxazine-4,4'-piperidin]-2(1H)-ones. | | Application | 2-Phenoxyethyl bromide can be used as a pharmaceutical intermediate for the synthesis of nafazodone and oxiperomide. | | Preparation | 2-Phenoxyethyl bromide is synthesized by the reaction of phenol and dibromoethane. Put phenol, dibromoethane and sodium hydroxide in a reaction pot and stir and mix, react at 110 °C for 6 hours, recover dibromoethane, the recovery amount is about 60%, wash with 5% sodium hydroxide solution and water, and divide Take the oil layer, distill under reduced pressure, and collect the fractions at 130-150°C (6.7kPa) to obtain (2-bromoethoxy)benzene. |
| 2-Phenoxyethylbromide Preparation Products And Raw materials |
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