1-ADAMANTYLOXYCARBONYL FLUORIDE

CAS No.：62087-82-5

Important Notice

This product is a chemical product/pharmaceutical intermediate. It is not a drug, an active pharmaceutical ingredient (API), or a pharmaceutical-grade material. It has not been granted a drug approval number or a Chemical Drug Substance Approval Notice, has not passed drug-related review and approval, and is not manufactured, tested, or released in accordance with pharmaceutical GMP.
This product is intended solely for non-clinical research, process development, quality studies, further chemical processing, or chemical synthesis. It must not be used in drug-product manufacturing, clinical trials, clinical diagnosis, or administration to humans or animals, or be sold, used as an input, submitted for regulatory filing, or released as an API or pharmaceutical material.
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1-ADAMANTYLOXYCARBONYL FLUORIDE Basic information

Product Name:	1-ADAMANTYLOXYCARBONYL FLUORIDE
Synonyms:	ADAMANTYL FLUOROFORMATE;ADOC-F;Fluoridocarbonic acid 1-adamantyl ester;Fluoroformic acid adamantan-1-yl ester;Fluoroformic acid tricyclo[3.3.1.13,7]decan-1-yl ester;1-ADAMANTYL FLUOROFORMATE;1-ADAMANTYLOXYCARBONYL FLUORIDE;1-ADOC-F
CAS:	62087-82-5
MF:	C11H15FO2
MW:	198.23
EINECS:	263-400-6
Product Categories:	Amine ProtectionProtection and Derivatization;Others;Peptide Synthesis;Protecting and Derivatizing Reagents;Specialty Synthesis
Mol File:	62087-82-5.mol

1-ADAMANTYLOXYCARBONYL FLUORIDE Chemical Properties

Melting point	30-32 °C (lit.)
Fp	192 °F
storage temp.	2-8°C
BRN	3590131

Safety Information

Hazard Codes	C
Risk Statements	34
Safety Statements	26-36/37/39-45
RIDADR	UN 2921 8/PG 1
WGK Germany	3

MSDS Information

Provider	Language
SigmaAldrich	English

1-ADAMANTYLOXYCARBONYL FLUORIDE Usage And Synthesis

Purification Methods

Dissolve it in n-hexane (ca 10g in 150 mL) and keep at 0o for 24hours. Any 1-adamantanol present will separate. Filter and evaporate to dryness. The crystalline residue has m 31-32o and is recrystallised from n-hexane (90g/500mL), (IR (KBr): max 1242, 1824 and 2340 cm-1). There should be no OH str band above 2500 cm-1. [Moroder et al. Hoppe-Seyler’s Z Physiol Chem 357 1647 1976, cf Haas et al. J Am Chem Soc 88 1988 1966.]

1-ADAMANTYLOXYCARBONYL FLUORIDE Preparation Products And Raw materials

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