Other grades of this product :
| 1-ADAMANTYLOXYCARBONYL FLUORIDE Basic information |
| 1-ADAMANTYLOXYCARBONYL FLUORIDE Chemical Properties |
| Melting point | 30-32 °C (lit.) | | Fp | 192 °F | | storage temp. | 2-8°C | | BRN | 3590131 |
| Hazard Codes | C | | Risk Statements | 34 | | Safety Statements | 26-36/37/39-45 | | RIDADR | UN 2921 8/PG 1 | | WGK Germany | 3 |
| 1-ADAMANTYLOXYCARBONYL FLUORIDE Usage And Synthesis |
| Purification Methods | Dissolve it in n-hexane (ca 10g in 150 mL) and keep at 0o for 24hours. Any 1-adamantanol present will separate. Filter and evaporate to dryness. The crystalline residue has m 31-32o and is recrystallised from n-hexane (90g/500mL), (IR (KBr): max 1242, 1824 and 2340 cm-1). There should be no OH str band above 2500 cm-1. [Moroder et al. Hoppe-Seyler’s Z Physiol Chem 357 1647 1976, cf Haas et al. J Am Chem Soc 88 1988 1966.] |
| 1-ADAMANTYLOXYCARBONYL FLUORIDE Preparation Products And Raw materials |
|
日本语
한국어
Français
Deutsch
España
Türkiye