Product

(R,R)-(+)-BIS(ALPHA-METHYLBENZYL)AMINE HYDROCHLORIDE

CAS No.：82398-30-9

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(R,R)-(+)-BIS(ALPHA-METHYLBENZYL)AMINE HYDROCHLORIDE Basic information

Product Name:	(R,R)-(+)-BIS(ALPHA-METHYLBENZYL)AMINE HYDROCHLORIDE
Synonyms:	[R-(R,R)]-(+)-BIS(ALPHA-METHYLBENZYL)AMINE HYDROCHLORIDE;(R,R)-(+)-BIS(ALPHA-METHYLBENZYL)AMINE HYDROCHLORIDE;(R,R)-(+)-BIS(1-PHENYLETHYL)AMINE HYDROCHLORIDE;(+)-BIS[(R)-1-PHENYLETHYL]AMINE HYDROCHLORIDE;(+)-BIS[(R)-ALPHA-METHYLBENZYL]AMINE HYDROCHLORIDE;(R,R)-(+)-Bis(α-methylbenzyl)amineHydrochloride;(R,R)-(+)-Bis(alpha-methylbenzyl)amineHCl;(+)-Bis[(R)-1-Phenylethyl]Amine HCl
CAS:	82398-30-9
MF:	C16H20ClN
MW:	261.79
EINECS:
Product Categories:	Amine SaltsAsymmetric Synthesis;Chiral Building Blocks;chiral;Chiral Resolution Reagents;Chiral Resolving Reagents;Organic Building Blocks;Asymmetric Synthesis;Synthetic Organic Chemistry
Mol File:	82398-30-9.mol

(R,R)-(+)-BIS(ALPHA-METHYLBENZYL)AMINE HYDROCHLORIDE Chemical Properties

Melting point	~260 °C
refractive index	73 ° (C=3, EtOH)
storage temp.	Inert atmosphere,Room Temperature
solubility	DMSO, Methanol
form	Solid
color	White
optical activity	[α]24/D +74°, c = 3 in ethanol
CAS DataBase Reference	82398-30-9(CAS DataBase Reference)

Safety Information

Hazard Codes	Xi,Xn
Risk Statements	36/37/38-22
Safety Statements	26-36/37/39
WGK Germany	3
F	3

MSDS Information

Provider	Language
ACROS	English
SigmaAldrich	English

(R,R)-(+)-BIS(ALPHA-METHYLBENZYL)AMINE HYDROCHLORIDE Usage And Synthesis

Chemical Properties	white to light yellow crystal powde
Uses	(αR)-α-Methyl-N-[(1R)-1-phenylethyl]benzenemethanamine Hydrochloride is used in the synthesis of the highly potent anti-metastatic prostacyclin analogue Cicaprost (C432750). Also used in the synthesis of a key A-Ring intermediate in the preparation of 1α-fluoro vitamin D3 analogues.

(R,R)-(+)-BIS(ALPHA-METHYLBENZYL)AMINE HYDROCHLORIDE Preparation Products And Raw materials

Raw materials	Ethyl acetate-->Tetrahydrofuran-->Dichloromethane-->Palladium-->Sodium borohydride-->Di-tert-butyl dicarbonate-->Acetophenone-->D-Tartaric acid-->(R)-(+)-1-Phenylethylamine
Preparation Products	(11AR)-(+)-10,11,12,13-TETRAHYDRODIINDENO[7,1-DE:1',7'-FG][1,3,2]DIOXAPHOSPHOCIN-5-BIS(R)-1PHENYLETHYL]AMINE

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