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| 1,3-Adamantanediamine Basic information |
| Product Name: | 1,3-Adamantanediamine | | Synonyms: | 1,3-Diaminoadamantane;1,3-Adamantanediamine;Tricyclo[3.3.1.13,7]decane-1,3-diamine;4. 1,3-diaminoadamantane;Tricyclo(3.3.1.1(sup 3,7))decane-1,3-diamine, dihydrochloride;(3-amino-1-adamantyl)amine dihydrochloride;13AD;1,3-Adamantanediaminewith2HClsalt | | CAS: | 10303-95-4 | | MF: | C10H18N2 | | MW: | 166.26 | | EINECS: | | Product Categories: | | Mol File: | 10303-95-4.mol |
| 1,3-Adamantanediamine Chemical Properties |
| Boiling point | 249 °C | | density | 1.153 | | Fp | 122 °C | | pka | 10.73±0.40(Predicted) | | form | powder to crystal | | color | White to Almost white | | CAS DataBase Reference | 10303-95-4(CAS DataBase Reference) |
| 1,3-Adamantanediamine Usage And Synthesis |
| Uses | 1,3-Adamantanediamine is used in preparation method of SSZ-13 molecular sieve from β molecular sieve. | | Preparation | 1,3-Adamantanediamine synthesis: 1,3-Adamantane dicarboxylic acid (12 g) was mixed with 50 mL of SOCl2 and the mixture was refluxed for 3 h. Excessive SOCl2 was evaporated and 1,3-adamantane dicarbonyl dichloride was obtained as white solid, dissolved in dried benzene and added to cold ammonia solution slowly, during which a white precipitate was formed gradually filtered and then washed the precipitate several times with water to give 1,3-disaminoacyladamantane as white solid, recrystallized from ethanol. White solid, yield 10.58 g (89 %). | | Purification Methods | Purify it by zone refining. The dibenzoyl derivative has m 248o, and the dihydrochloride salt has m 310o (360o) after recrystallisation from aqueous EtOH or EtOH/Et2O. [Prelog & Seiwerth Chem Ber 74 1769 1941, Stetter & Wulff Chem Ber 93 1366 1960.] |
| 1,3-Adamantanediamine Preparation Products And Raw materials |
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