(9-phenyl-9H-carbazol-2-yl)boronic acid

(9-phenyl-9H-carbazol-2-yl)boronic acid
  • CAS No.:1001911-63-2
Other grades of this product :
(9-phenyl-9H-carbazol-2-yl)boronic acid Basic information
Product Name:(9-phenyl-9H-carbazol-2-yl)boronic acid
Synonyms:9-Phenylcarbazole-2-boronic acid;B-(9-Phenyl-9H-carbazol-2-yl)-boronic acid;(9-phenyl-9H-carbazol-2-yl)boronic acid (2PCBA);2-BAPC;9-Phenylcarbazole-2-boronic Acid (contains varying amounts of Anhydride);(9-phenyl-9H-carbazol-2-yl)boronic acid;Boronic acid,B-(9-phenyl-9H-carbazol-2-yl)-;(9-phenylcarbazol-2-yl)boronic Acid
CAS:1001911-63-2
MF:C18H14BNO2
MW:287.12
EINECS:
Product Categories:
Mol File:1001911-63-2.mol
(9-phenyl-9H-carbazol-2-yl)boronic acid Chemical Properties
Boiling point 466.0±51.0 °C(Predicted)
density 1.20±0.1 g/cm3(Predicted)
storage temp. under inert gas (nitrogen or Argon) at 2-8°C
solubility very slightly in Tetrahydrofuran
pka8.91±0.30(Predicted)
form powder to crystal
color White to Almost white
Safety Information
HS Code 2931900090
MSDS Information
(9-phenyl-9H-carbazol-2-yl)boronic acid Usage And Synthesis
Uses(9-phenyl-9H-carbazol-2-yl)boronic acid can be used as an intermediate in organic synthesis, mainly used in laboratory research and development and in the process of chemical and pharmaceutical synthesis.
SynthesisSub 1-3-1 (6.4g, 20mmol) was dissolved in anhydrous Ether, lowering the temperature of the reaction to -78°C, n-BuLi (2.5M in hexane) (1.4g, 22mmol) was added dropwise slowly, and after, the reaction It was stirred for 30 minutes. After lowering the temperature of the reaction back to -78°C dropwise Triisopropyl borate (5.6g, 30mmol). Stirring at room temperature, diluted with water and it binds the 2N HCl. After completion of reaction, ethyl acetate and water, dried over MgSO4 and the organic layer was extracted and recrystallized silicagel column and the resulting organic material and then concentrated to a Sub 1-4-1 4.5g (yield: 78%) was obtained.
(9-phenyl-9H-carbazol-2-yl)boronic acid Preparation Products And Raw materials
Preparation Products5,11-dihydro-5-phenylindolo[3,2-b]carbazole

Welcome!

Please leave a message for us or use the following ways to contact us, we will reply to you as soon as possible, and provide you with the most sincere service, thank you.

  • NO. 18 ,Wujiang Road, Wulidian Street, Jiangbei District, Chongqing
  • +86-23-6139-8061 +86-13650506873
  • danny@chemdad.com sales@chemdad.com
  • www.chemdad.com
  • WhatsApp +86-13650506873

Name

phone

company

email

message

Payment methods
Google translate: 日本语日本语 한국어한국어 FrançaisFrançais DeutschDeutsch EspañaEspaña TürkiyeTürkiye