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| 4-BroMo-9H-carbazole Basic information |
| Product Name: | 4-BroMo-9H-carbazole | | Synonyms: | 4-BroMo-9H-carbazole;4-broMocarbazole;4-BroMo-9H-carbazole
(4BC);9H-Carbazole, 4-broMo-;Carb;1-CYCLOPROPYL-2,6-PIPERAZINEDIONE;Carbazole, 4-bromo-;4-Bromocarbazole > | | CAS: | 3652-89-9 | | MF: | C12H8BrN | | MW: | 246.1 | | EINECS: | 810-963-6 | | Product Categories: | OLED | | Mol File: | 3652-89-9.mol |
| 4-BroMo-9H-carbazole Chemical Properties |
| Melting point | 104-105℃ | | Boiling point | 409.2±18.0 °C(Predicted) | | density | 1.617±0.06 g/cm3 (20 ºC 760 Torr) | | storage temp. | Sealed in dry,Room Temperature | | form | powder to crystal | | pka | 16.04±0.30(Predicted) | | color | White to Light yellow | | InChIKey | CBJHFGQCHKNNJY-UHFFFAOYSA-N |
| 4-BroMo-9H-carbazole Usage And Synthesis |
| Chemical Properties | White powder. | | Uses | 4-BROMO-9H-CARBAZOLE is a useful research chemical. | | Synthesis | Under nitrogen protection,Add 357.6g m-dibromobenzene (99%, 1.5mol) into a 500mL reaction flask,26.1g o-bromoaniline (99%, 0.15mol),0.084g palladium(II) acetate (99%, 0.375mmol),0.18g 2-dicyclohexylphosphine-2,4,6-triisopropylbiphenyl (99%, 0.375mmol),58.2g sodium tert-butoxide (99%, 0.6mol),After feeding,Warm up to 130°C,Stirring speed 600rpm,Incubate for 24hr,After the reaction,Vacuum distillation to recover unreacted m-dibromobenzene,Add water and ethyl acetate to extract the residue,The organic layer was desolvated to obtain the crude product which was crystallized in ethanol to obtain 34.3 g of 4-BroMo-9H-carbazole.The content is 99.6% and the yield is 92.5%. |
| 4-BroMo-9H-carbazole Preparation Products And Raw materials |
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