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| 1-bromodibenzo[b,d]furan Basic information |
| Product Name: | 1-bromodibenzo[b,d]furan | | Synonyms: | 1-Bromodibenzo[b,d]fur;1-Brom-dibenzofuran;Dibenzofuran, 1-broMo-;1-Bromodibenzofuran;1-BroModibenzo[b,d]furan;-Bromodibenzo[b,d]furan;1-BDPF;1-bromo-dibenzofuran（1-BDPF） | | CAS: | 50548-45-3 | | MF: | C12H7BrO | | MW: | 247.09 | | EINECS: | | Product Categories: | oled | | Mol File: | 50548-45-3.mol |
| 1-bromodibenzo[b,d]furan Chemical Properties |
| Melting point | 67℃ | | Boiling point | 343.8±15.0 °C(Predicted) | | density | 1.577±0.06 g/cm3(Predicted) | | storage temp. | Sealed in dry,Room Temperature | | form | powder to crystal | | color | White to Gray to Brown |
| 1-bromodibenzo[b,d]furan Usage And Synthesis |
| Uses | 1-bromodibenzo[b,d]furan can be used as organic synthesis intermediates and pharmaceutical intermediates, mainly used in laboratory research and development and chemical and pharmaceutical production processes. | | Synthesis | 111 g (416 mmol) of 6’-bromo-2’-fluorobiphenyl-2-ol are dissolved in 21 of SeccoSolv DMF (max 0.003% of H20) and cooled to 5°C. 20 g (449 mmol) of sodium hydride (60% suspension in paraffin oil) are added in portions tothis solution, and the mixture is stirred for a further 20 mm. after the addition is complete and then heated at 100°C for 45 mm. After cooling, 500 ml of ethanol are slowly added to the mixture, which is then evaporated to dryness in a rotary evaporator and purified by chromatography. Yield: 90 g (367 mmol), 88.5% of theory. |
| 1-bromodibenzo[b,d]furan Preparation Products And Raw materials |
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![1-bromodibenzo[b,d]furan](/img/50548-45-3.jpg "1-bromodibenzo[b,d]furan")
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