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| 1,4,10,13-TETRAOXA-7,16-DIAZACYCLOOCTADECANE Basic information |
| Product Name: | 1,4,10,13-TETRAOXA-7,16-DIAZACYCLOOCTADECANE | | Synonyms: | 1,4,10,13-TETRAOXA-7,16-DIAZACYCLOOCTADECANE;1,10-DIAZA-18-CROWN-6;KRYPTOFIX 22 POLYMER (SILICA GEL) FOR SYNTHESIS;Diaza-18-crown-6,98%;Diaza-18-crown-6, 98% 500MG;KRYPTOFIX 22 FOR SYNTHESIS;4,13-DIAZA-18-CROWN-6;4,13-DIAZA-18-CROWN 6-ETHER | | CAS: | 23978-55-4 | | MF: | C12H26N2O4 | | MW: | 262.35 | | EINECS: | 245-965-0 | | Product Categories: | Azacrown Ethers;Crown Ethers;Functional Materials;Macrocycles for Host-Guest Chemistry | | Mol File: | 23978-55-4.mol |
| 1,4,10,13-TETRAOXA-7,16-DIAZACYCLOOCTADECANE Chemical Properties |
| Melting point | 111-114 °C(lit.) | | Boiling point | 405.6°C (rough estimate) | | density | 1.0807 (rough estimate) | | refractive index | 1.4560 (estimate) | | storage temp. | Store below +30°C. | | form | Shiny Crystalline Powder | | pka | 9.00±0.20(Predicted) | | color | Off-white | | Water Solubility | Soluble in water. | | BRN | 609764 | | CAS DataBase Reference | 23978-55-4(CAS DataBase Reference) |
| Hazard Codes | Xi | | Risk Statements | 36/37/38 | | Safety Statements | 26-37/39-37 | | WGK Germany | 2 | | RTECS | HM1650000 | | F | 10 | | HS Code | 2934 99 90 | | Toxicity | LD50 orally in Rabbit: 3400 mg/kg |
| 1,4,10,13-TETRAOXA-7,16-DIAZACYCLOOCTADECANE Usage And Synthesis |
| Chemical Properties | off-white shiny crystalline powder | | Uses | 1,4,10,13-Tetraoxa-7,16-diazacyclooctadecane is a crown ether, which can be used:- In the spectroscopic studies of its complex-forming reaction with iodine.
- To prepare the ligand 7,16-bis(5-t-butyl-2-hydroxybenzyl)-1,4,10,13-tetraoxa-7,16-diazacyclooctadecane.
- As a ligand in the study of zirconium facilitated hydrolysis of a dipeptide at neutral pH.
| | Purification Methods | Twice recrystallise it from *benzene/n-heptane, and dry it for 24hours under high vacuum [Weber & V.gtle Top Curr Chem (Springer Verlag, Berlin) 98 1 1981, D'Aprano & Sesta J Phys Chem 91 2415 1987]. |
| 1,4,10,13-TETRAOXA-7,16-DIAZACYCLOOCTADECANE Preparation Products And Raw materials |
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