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| 2-Amino-5-chlorobenzonitrile Basic information |
| 2-Amino-5-chlorobenzonitrile Chemical Properties |
| Melting point | 96-99 °C (lit.) | | Boiling point | 132-135 °C/0.5 mmHg (lit.) | | density | 1.2763 (rough estimate) | | refractive index | 1.5500 (estimate) | | Fp | >230 °F | | storage temp. | Keep in dark place,Inert atmosphere,Room temperature | | solubility | Chloroform (Slightly), DMSO (Slightly) | | form | Crystalline Needles | | pka | 1.18±0.10(Predicted) | | color | White to light beige | | CAS DataBase Reference | 5922-60-1(CAS DataBase Reference) | | EPA Substance Registry System | Benzonitrile, 2-amino-5-chloro- (5922-60-1) |
| Hazard Codes | Xn,Xi | | Risk Statements | 20/21/22-36/37/38 | | Safety Statements | 26-36-36/37/39 | | RIDADR | 3276 | | WGK Germany | 3 | | Hazard Note | Irritant | | TSCA | Yes | | HazardClass | 6.1 | | PackingGroup | III | | HS Code | 29269090 |
| 2-Amino-5-chlorobenzonitrile Usage And Synthesis |
| Chemical Properties | white to light beige crystalline needles | | Uses | 2-Amino-5-chlorobenzonitrile was used to build up the 2,2-dioxide-1H-2,1,3-benzothiadiazine ring system. | | Preparation | Synthesis of 2-amino-5-chlorobenzonitrile is reported in the literature by two methods. The first method involves synthesis from 2-aminobenzonitrile, N-chlorosuccinimide an d acetonitrile. The second method involves synthesis from 5-chloroisatin-β-oxime and bis(2-ethylhexyl)phthalate. Both the methods are not feasible commercially as far as the cost and availability of raw materials are concerned. | | Synthesis Reference(s) | Synthetic Communications, 20, p. 71, 1990 DOI: 10.1080/00397919008054617 | | General Description | The vibrational spectra of 2-amino-5-chlorobenzonitrile was studied using density functinal theory. |
| 2-Amino-5-chlorobenzonitrile Preparation Products And Raw materials |
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