4-Methoxyphenylmagnesium bromide

CAS No.：13139-86-1

Important Notice

This product is a chemical product/pharmaceutical intermediate. It is not a drug, an active pharmaceutical ingredient (API), or a pharmaceutical-grade material. It has not been granted a drug approval number or a Chemical Drug Substance Approval Notice, has not passed drug-related review and approval, and is not manufactured, tested, or released in accordance with pharmaceutical GMP.
This product is intended solely for non-clinical research, process development, quality studies, further chemical processing, or chemical synthesis. It must not be used in drug-product manufacturing, clinical trials, clinical diagnosis, or administration to humans or animals, or be sold, used as an input, submitted for regulatory filing, or released as an API or pharmaceutical material.
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4-Methoxyphenylmagnesium bromide Basic information

Product Name:	4-Methoxyphenylmagnesium bromide
Synonyms:	4-Methoxyphenylmagnesium Bromide 1.0 M In Tetrahydrofuran;4-METHOXYPHENYLMAGNESIUM BROMIDE 0.5 M IN THF;4-Methoxyphenylmagnesium bromide, 1M solution in THF;4-anisylmagnesium bromide, 0.5m in thf;4-Methoxyphenylmagnesium bromide1M solution in THFAcroSeal§3;(4-Methoxyphenyl)bromomagnesium;4-Methoxyphenylbromomagnesium;p-Anisylbromomagnesium
CAS:	13139-86-1
MF:	C7H7BrMgO
MW:	211.34
EINECS:
Product Categories:	Chemical Synthesis;Grignard Reagents;Aryl;Grignard Reagents;Organometallic Reagents;Organometallic Reagents
Mol File:	13139-86-1.mol

4-Methoxyphenylmagnesium bromide Chemical Properties

Boiling point	65-67 °C
density	0.955 g/mL at 25 °C
Fp	−4 °F
storage temp.	Flammables + water-Freezer (-20°C)e area
form	Liquid
color	Yellow to brown
Water Solubility	Severe reaction
Sensitive	Air & Moisture Sensitive
Exposure limits	ACGIH: TWA 50 ppm; STEL 100 ppm (Skin)OSHA: TWA 200 ppm(590 mg/m3)NIOSH: IDLH 2000 ppm; TWA 200 ppm(590 mg/m3); STEL 250 ppm(735 mg/m3)

Safety Information

Hazard Codes	F,C
Risk Statements	11-14-19-22-34-14/15-40-37
Safety Statements	16-26-33-36/37/39-45-6A-43B
RIDADR	UN 2924 3/PG 2
WGK Germany	-
HazardClass	4.3
PackingGroup	II
HS Code	29319090

MSDS Information

Provider	Language
ACROS	English
SigmaAldrich	English

4-Methoxyphenylmagnesium bromide Usage And Synthesis

Chemical Properties	Clear to brown solution when properly stored
Uses	4-Methoxyphenylmagnesium bromide is applied in Grignard-reactions as a reagent for the introduction of the 4-methoxyphenyl group.

4-Methoxyphenylmagnesium bromide Preparation Products And Raw materials

Preparation Products

(4-METHOXYPHENYL)DIPHENYLSULFONIUM TRIFLATE-->4-METHOXYPHENETHYL BROMIDE-->4,4'-DIMETHOXYBENZHYDROL-->4-Methoxybiphenyl-->4'-METHOXY-2,2,2-TRIFLUOROACETOPHENONE-->4-METHOXYAZOBENZENE-->Bis(4-methoxyphenyl)phosphine oxide-->4-Methoxytriphenylchloromethane

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