Disperse Blue 14

Disperse Blue 14
  • CAS No.:2475-44-7
Other grades of this product :
Disperse Blue 14 Basic information
Description
Product Name:Disperse Blue 14
Synonyms:1,4-BIS(METHYLAMINO)ANTHRAQUINONE;C.I. 61500~Disperse Blue 14;Disperse Blue?4;Solvent Blue 59:1;C.I.DISPERSEBLUE14;ANTHRAQUINONE,1,4-BIS(METHYLAMINO)-;Oil Blue 78;9,10-Anthracenedione, 1,4-bis(methylamino)-
CAS:2475-44-7
MF:C16H14N2O2
MW:266.29
EINECS:219-602-1
Product Categories:Solvent Dyestuff;Aminoanthraquinones;Anthraquinones
Mol File:2475-44-7.mol
Disperse Blue 14 Chemical Properties
Melting point 220-222°C
Boiling point 409.5°C (rough estimate)
density 1.1262 (rough estimate)
refractive index 1.6240 (estimate)
storage temp. Keep in dark place,Inert atmosphere,Room temperature
solubility soluble in Alcohol,Acetone,Toluene,Nitrobenzene
form Powder
pka5.78±0.20(Predicted)
Colour Index 61500
color Dark purple
Water Solubility 37.28ug/L(25 ºC)
BRN 2220693
CAS DataBase Reference2475-44-7(CAS DataBase Reference)
EPA Substance Registry System9,10-Anthracenedione, 1,4-bis(methylamino)- (2475-44-7)
Safety Information
Hazard Codes Xi
Risk Statements 36/37/38
Safety Statements 26-36
WGK Germany 3
RTECS CB5750000
TSCA Yes
HS Code 29147000
MSDS Information
ProviderLanguage
1,4-Bis(methylamino)anthraquinone English
ALFA English
Disperse Blue 14 Usage And Synthesis
DescriptionDisperse blue 14 is also known as transparent blue GP. Its chemical name is 1,4-bis(methylamino)anthraquinone. It is a blue-black powder, insoluble in water, soluble in methanol, ethanol, glacial acetic acid, nitrobenzene, pyridine and toluene. It is reddish brown in concentrated sulfuric acid.
Preparation1,4-Dihydroxyanthracene-9,10-dione?by under pressure,?With aqueous Methanamine?and sodium hydrosulfite or zinc processing. Leuco sulfate nitrobenzene oxidation or thermal
Properties and Applicationsbright blue. Blue powder. Soluble in acetone, glacial acetic acid, the difficulties, pyridine and toluene. The strong sulfuric acid to red light brown. Used for polyester, vinegar and polyamide fiber dyeing, also can be used to transfer printing. And is fit for manufacturing fireworks fireworks hair color components. Can also be used in such of surface colouring and plastic.
Standard(Polyamide) Ironing Fastness Light Fastness Persperation Fastness Washing Fastness
Fading Stain Fading Stain Fading Stain
ISO 4 2-3 4-5 4-5 2-3 4 3-4
Purification MethodsPurify the anthraquinone by thin-layer chromatography on silica gel plates, using toluene/acetone (3:1) as eluent. The main band is scraped off and extracted with MeOH. The solvent is evaporated and the dye is dried in a drying pistol [Land et al. J Chem Soc, Faraday Trans 1 72 2091 1976]. It crystallises from n-butanol with m 221-222o and has max 539 and 644nm (EtOH). [Beilstein 14 H 198, 14 III 440, 14 IV 459.]

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