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| 1,3-Dibromobenzene Basic information |
| 1,3-Dibromobenzene Chemical Properties |
| Melting point | -7 °C (lit.) | | Boiling point | 218-219 °C (lit.) | | density | 1.952 g/mL at 25 °C (lit.) | | vapor density | 8.16 (vs air) | | vapor pressure | 5 mm Hg ( 66 °C) | | refractive index | n20/D 1.608(lit.) | | Fp | 201 °F | | storage temp. | Sealed in dry,Room Temperature | | solubility | 0.068g/l | | form | Liquid | | Specific Gravity | 1.952 | | color | Clear colorless to light yellow | | Water Solubility | insoluble | | BRN | 1904538 | | CAS DataBase Reference | 108-36-1(CAS DataBase Reference) | | NIST Chemistry Reference | Benzene, 1,3-dibromo-(108-36-1) | | EPA Substance Registry System | m-Dibromobenzene (108-36-1) |
| Hazard Codes | Xi,C | | Risk Statements | 36/37/38 | | Safety Statements | 26-36-24/25 | | RIDADR | UN 2711 | | WGK Germany | 2 | | RTECS | CZ1790000 | | Hazard Note | Irritant | | TSCA | T | | HazardClass | 3.2 | | PackingGroup | III | | HS Code | 29036990 |
| 1,3-Dibromobenzene Usage And Synthesis |
| Chemical Properties | clear colourless to light yellow liquid | | Uses | 1,3-Dibromobenzene is used in Suzuki coupling reaction for the preparation of [n]metacyclophanes. It is used to prepare 5-(3-bromo-phenyl)-2,4-di-tert-butoxy-pyrimidine using Pd(0) (PPh3)4 as a reagent. Further, it undergoes solid-supported potassium fluoride-aluminum oxide palladium-catalyzed polyarylation reaction with phenyl boronic acid to get conjugated polyaryls. | | Definition | ChEBI: A dibromobenzene carrying bromo groups at positions 1 and 3. | | General Description | 1,3-Dibromobenzene undergoes solid-supported [KF-Al2O3] palladium-catalyzed polyarylation reaction with phenyl boronic acid under microwave irradiation to yield conjugated polyaryls. |
| 1,3-Dibromobenzene Preparation Products And Raw materials |
| Raw materials | 3-Bromoaniline | | Preparation Products | 3-MORPHOLINOPHENYLBORONIC ACID PINACOL ESTER-->2-Bromoanthracene-->(3-Bromophenyl)triphenylsilane-->Benzene, 1,1'-(diphenylsilylene)bis[3-bromo--->Benzene, 1,5-dibromo-2,4-diiodo--->3,5-Dibromoaniline-->3-(9H-Carbazol-9-yl)phenylboronic acid-->1-Hydroxy-8-bromonaphthalene-->1-BROMO-8-METHYLNAPHTHALENE-->(2,6-DibroMophenyl)Methanol-->3-BROMO-4'-CHLOROBENZOPHENONE-->2,4,6-TRIBROMOBENZOIC ACID-->2,2',4,4'-TETRABROMODIPHENYL ETHER-->1,3-DIBROMO-4-IODOBENZENE-->FLUCONAZOLE IMPURITY C-->3-PHENOXYBROMOBENZENE |
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