Product

BORANE-N,N-DIETHYLANILINE COMPLEX

CAS No.：13289-97-9

Other grades of this product :

BORANE-N,N-DIETHYLANILINE COMPLEX Basic information

Product Name:	BORANE-N,N-DIETHYLANILINE COMPLEX
Synonyms:	BORANE-N,N-DIETHYLANILINE;BORANE-N,N-DIETHYLANILINE COMPLEX;N,N-DIETHYLANILINE BORANE;n,n-diethylanilineborane,deanb;n-diethylbenzenamine)trihydro-((beta-4)-boro;(N,N-diethylaniline)trihydroboron;Borane-N,N-diethylaniline complex,97%;N, N diethylaniline borane complex
CAS:	13289-97-9
MF:	C10H18BN
MW:	163.07
EINECS:	236-305-2
Product Categories:	B (Classes of Boron Compounds);Boranes;Reduction;Synthetic Organic Chemistry;Synthetic Reagents
Mol File:	13289-97-9.mol

BORANE-N,N-DIETHYLANILINE COMPLEX Chemical Properties

Melting point	−30-−27 °C(lit.)
density	0.917 g/mL at 25 °C(lit.)
refractive index	1.5245-1.5265
Fp	70 °F
storage temp.	Refrigerator
form	Liquid
color	Clear colorless to yellow
Water Solubility	MAY DECOMPOSE
InChIKey	YPWBYWNNJVSNPQ-UHFFFAOYSA-N
CAS DataBase Reference	13289-97-9(CAS DataBase Reference)
EPA Substance Registry System	Boron, (N,N-diethylbenzenamine)trihydro-, (T-4)- (13289-97-9)

Safety Information

Risk Statements	10-14-51/53-33-23/24/25-14/15
Safety Statements	16-33-36/37/39-43-9-61-45-28A-8
RIDADR	UN 3398 4.3/PG 2
WGK Germany	3
HazardClass	3.1
PackingGroup	II
HS Code	29299090

MSDS Information

Provider	Language
SigmaAldrich	English
ACROS	English

BORANE-N,N-DIETHYLANILINE COMPLEX Usage And Synthesis

Chemical Properties

clear colorless to amber liquid

Uses

Reactant for:

Diastereoselective reduction of prochiral enone intermediates
Borylation of aryl halides
Reductions of ketones, acids, esters, amides, and nitriles
Investigations of borane source on enantioselectivity in enantiopure oxazaborolidine-catalyzed asymmetric borane reduction of ketones

Reactant for synthesis of:

Chromanol derivatives as CETP inhibitors for the treatment of cardiovascular disease
Allylic alcohols via enantioselective reductions
Pinacolboranes for one-pot synthesis of unsymmetrical biaryls

BORANE-N,N-DIETHYLANILINE COMPLEX Preparation Products And Raw materials

Raw materials

N,N-DIETHYLANILINE HYDROCHLORIDE-->Borane-tetrahydrofuran complex-->Diborane-->Sodium borohydride-->N,N-Diethylaniline-->Tributyltin Hydride-->Boron trichloride

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