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| 3,5-Bis(trifluoromethyl)aniline Basic information |
| Product Name: | 3,5-Bis(trifluoromethyl)aniline | | Synonyms: | ,,,’,’,’-Hexafluoro-3,5-xylidine;,5-Bis-trifluoromethyl-phenylamine;,5-Xylidine, a,a,a,a',a',a'-hexafluoro-;,a,a,a',a',a'-Hexafluoro-3,5-xylidine;3,5-bis(trifluoromethyl)-anilin;3,5-bis(trifluoromethyl)-benzenamin;3,5-Bis(trifluoromethyl)benzenamine;3,5-Di(trifluorometh | | CAS: | 328-74-5 | | MF: | C8H5F6N | | MW: | 229.12 | | EINECS: | 206-335-0 | | Product Categories: | Aniline series;Fluorobenzene;Trifluoromethylbenzene serise;Anilines, Aromatic Amines and Nitro Compounds;Miscellaneous | | Mol File: | 328-74-5.mol |
| 3,5-Bis(trifluoromethyl)aniline Chemical Properties |
| Hazard Codes | Xi,Xn | | Risk Statements | 33-36/37/38-20/21/22 | | Safety Statements | 26-36/37/39-36 | | RIDADR | 2810 | | WGK Germany | 3 | | RTECS | ZE9800000 | | Hazard Note | Irritant | | TSCA | Yes | | HazardClass | 6.1 | | PackingGroup | III | | HS Code | 29214910 |
| 3,5-Bis(trifluoromethyl)aniline Usage And Synthesis |
| Chemical Properties | clear light yellow to yellow-brown liquid | | Uses | 3,5-Bis(trifluoromethyl)aniline was found to be a highly efficient monodentate transient directing group (MonoTDG) for the palladium-catalyzed direct dehydrogenative cross-coupling of benzaldehydes with arenes. | | Synthesis | The synthesis of 3,5-Bis(trifluoromethyl)aniline is as follows is as follows：Put 259g (1mol) 3,5-Bis(trifluoromethyl)nitrobenzeneand 500g ethyl acetate into a 1L autoclave, add 5g palladium-carbon as a catalyst, raise the temperature to 60℃, then pass the hydrogen pressure to 2MPa, keep the temperature and react for 20 hours, then cooling, filtration, concentration, and distillation to obtain 3,5-Bis(trifluoromethyl)aniline with a purity of 98.5% and a yield of 87%. |
| 3,5-Bis(trifluoromethyl)aniline Preparation Products And Raw materials |
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