Product

2-Amino-6-methylpyridine

CAS No.：1824-81-3

Other grades of this product :

2-Amino-6-methylpyridine Basic information

Product Name:	2-Amino-6-methylpyridine
Synonyms:	2-amino-6-methyl-pyridin;2-Picoline, 6-amino-;2-Pyridinamine,6-methyl-;6-Amino-2-methylpyridine;6-Methyl-2-aminopyridine;2-AMINO-6-METHYL PYRIDINE 6-METHYLPYRIDIN-2-YLAMINE;2-AMINO-6-METHYLPYRIDINE (2-AMINO-6-PICOLINE);2-Amino-6-picoline ,98%
CAS:	1824-81-3
MF:	C6H8N2
MW:	108.14
EINECS:	217-360-1
Product Categories:	VARIOUSAMINE;Pyridine;Pyridines, Pyrimidines, Purines and Pteredines;Pyridines derivates;Heterocycle-Pyridine series
Mol File:	1824-81-3.mol

2-Amino-6-methylpyridine Chemical Properties

Melting point	40-44 °C(lit.)
Boiling point	208-209 °C(lit.)
density	1.0275 (estimate)
refractive index	1.5560 (estimate)
Fp	218 °F
storage temp.	Keep in dark place,Inert atmosphere,Room temperature
pka	pK1: 7.41(+1) (25°C)
form	Crystalline Low Melting Solid
color	Yellow
Water Solubility	very faint turbidity
Sensitive	Hygroscopic
BRN	107048
InChIKey	QUXLCYFNVNNRBE-UHFFFAOYSA-N
CAS DataBase Reference	1824-81-3(CAS DataBase Reference)
NIST Chemistry Reference	2-Pyridinamine, 6-methyl-(1824-81-3)
EPA Substance Registry System	2-Pyridinamine, 6-methyl- (1824-81-3)

Safety Information

Hazard Codes	T
Risk Statements	25-36/37/38-24/25-23/24/25-24
Safety Statements	26-36/37/39-45-37/39-28A
RIDADR	UN 2811 6.1/PG 3
WGK Germany	3
RTECS	US1885000
F	10-21
TSCA	Yes
HazardClass	6.1
PackingGroup	II
HS Code	29333999

MSDS Information

Provider	Language
2-Amino-6-methylpyridine	English
SigmaAldrich	English
ACROS	English
ALFA	English

2-Amino-6-methylpyridine Usage And Synthesis

Chemical Properties	YELLOWISH CRYSTALLINE LOW MELTING SOLID
Uses	Intermediate.
Purification Methods	Crystallise it three times from acetone and dry it under vacuum at ca 45o. Alternatively, keep it in contact with NaOH pellets for 3hours, with occasional shaking, decant and fractionally distil it [Mod et al. J Phys Chem 60 1651 1956]. It also recrystallises from CH2Cl2 on addition of pet ether. [Marzilli et al. J Am Chem Soc 108 4830 1986, Beilstein 22/9 V 210.]

2-Amino-6-methylpyridine Preparation Products And Raw materials

Raw materials

Sodium-->Ammonia-->4-Chlorobenzaldehyde-->2-Picoline-->Ferric nitrate

Preparation Products

3-AMINO-2-METHOXY-6-PICOLINE-->3-BROMO-6-CHLORO-2-METHYL-5-NITROPYRIDINE-->3-BROMO-6-METHOXY-2-METHYL-5-NITROPYRIDINE-->3-Amino-6-methoxypyridine-2-carboxylic acid-->2-FLUORO-6-METHYLPYRIDINE-3-BORONIC ACID-->2-Amino-6-methyl-5-nitropyridine-->3-Amino-6-chloro-2-picoline-->3,6-DICHLORO-4-HYDROXYPYRIDINE-2-CARBOXYLIC ACID-->5-BROMO-3-NITRO-6-METHYLPYRIDIN-2(1H)-ONE-->2-CHLORO-5-FLUOROPYRIDINE-6-CARBOXYLIC ACID-->2-ISOCYANATO-6-NITROPYRIDINE-->2-Amino-5-bromo-6-methylpyridine-->6-AMINO-3-BROMO-2-METHYL-5-NITRO-PYRIDINE-->6-METHYL-PYRIDINE-2,5-DIAMINE-->2-Amino-6-nitropyridine-->6-Methylpyridine-2-carbonitrile-->6-NITROPYRIDINE-2-CARBOXAMIDE-->6-NITROPYRIDINE-2-CARBOXYLIC ACID ETHYL ESTER-->6-TERT-BUTOXYCARBONYLAMINO-PYRIDINE-2-CARBOXYLIC ACID-->6-NITROPYRIDINE-2-CARBOXYLIC ACID-->2-Hydroxy-6-methyl-5-nitropyridine-->2-Amino-3-nitro-6-picoline-->6-METHYLPYRIDINE-2-BORONIC ACID-->3-BROMO-6-HYDROXY-2-METHYLPYRIDINE-->6-NITROPYRIDINE-2-CARBONYL CHLORIDE-->2-FLUORO-6-PYRIDINECARBONYL CHLORIDE-->2-Fluoropyridine-6-carboxylic acid-->2-AMINO-3,5-DICHLORO-6-METHYLPYRIDINE-->2-Fluoro-6-methylpyridine-->6-(ACETYLAMINO)-2-PYRIDINECARBOXYLIC ACID

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