Other grades of this product :
| 3-Nitroacetophenone Basic information |
| 3-Nitroacetophenone Chemical Properties |
| Melting point | 76-78 °C(lit.) | | Boiling point | 202 °C(lit.) | | density | 1.3450 (rough estimate) | | vapor pressure | 0.32Pa at 25℃ | | refractive index | 1.5468 (estimate) | | Fp | 202°C | | storage temp. | Sealed in dry,Room Temperature | | solubility | DMSO (Slightly), Methanol (Slightly) | | form | Crystalline Powder | | color | Yellow to yellow-green | | Odor | Odorless | | Water Solubility | <0.01 g/100 mL at 20 ºC | | BRN | 743002 | | Stability: | Stable. Incompatible with strong oxidizing agents, strong bases. | | InChIKey | ARKIFHPFTHVKDT-UHFFFAOYSA-N | | LogP | 1.42 | | NIST Chemistry Reference | 3-Nitroacetophenone(121-89-1) | | EPA Substance Registry System | 3-Nitroacetophenone (121-89-1) |
| 3-Nitroacetophenone Usage And Synthesis |
| Chemical Properties | white to light beige crystalline powder or yellow needle-like crystals. soluble in hot water and ether, slightly soluble in ethanol. can be volatile with water vapor. | | Uses | 3''-Nitroacetophenone is used as a reactant in the synthesis of fluorine based aminothiazoles with antimicrobial activity. | | Uses | 3′-Nitroacetophenone can undergo high hydrostatic pressure-assisted reduction with Ni–Al alloy in water to form 1-(3-aminophenyl)ethanol. | | Preparation | 3-Nitroacetophenone is synthesized from acetophenone by nitration.Synthesis of 3-nitroacetophenone | | General Description | 3-nitroacetophenone is a light beige powder. It is an anthropogenic compound which is used as a synthetic intermediate in the production of dyes and other organic compounds. (NTP, 1992) | | Air & Water Reactions | Insoluble in water. | | Reactivity Profile | A nitrated ketone. Ketones are reactive with many acids and bases liberating heat and flammable gases (e.g., H2). The amount of heat may be sufficient to start a fire in the unreacted portion of the ketone. Ketones react with reducing agents such as hydrides, alkali metals, and nitrides to produce flammable gas (H2) and heat. Ketones are incompatible with isocyanates, aldehydes, cyanides, peroxides, and anhydrides. They react violently with aldehydes, HNO3, HNO3 + H2O2, and HClO4. | | Fire Hazard | Flash point data for 3-Nitroacetophenone are not available, however 3-Nitroacetophenone is probably combustible. | | Purification Methods | Distil the ketone in steam and crystallise it from EtOH. [Beilstein 7 IV 656.] |
| 3-Nitroacetophenone Preparation Products And Raw materials |
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