Ethyl p-nitrobenzoate

CAS No.：99-77-4

Important Notice

This product is a chemical product/pharmaceutical intermediate. It is not a drug, an active pharmaceutical ingredient (API), or a pharmaceutical-grade material. It has not been granted a drug approval number or a Chemical Drug Substance Approval Notice, has not passed drug-related review and approval, and is not manufactured, tested, or released in accordance with pharmaceutical GMP.
This product is intended solely for non-clinical research, process development, quality studies, further chemical processing, or chemical synthesis. It must not be used in drug-product manufacturing, clinical trials, clinical diagnosis, or administration to humans or animals, or be sold, used as an input, submitted for regulatory filing, or released as an API or pharmaceutical material.
The purchaser must not use this product, or supply it to another party, for personal consumption, sports or fitness, weight loss, health supplements, food, or animal feed.

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Ethyl p-nitrobenzoate Basic information

Product Name:	Ethyl p-nitrobenzoate
Synonyms:	4-(ethoxycarbonyl)nitrobenzene;4-nitro-benzoicaciethylester;Benzoic acid, 4-nitro-, ethyl ester;Benzoic acid, p-nitro-, ethyl ester;Ethyl nitrobenzoate, para ester;Ethyl para-nitrobenzoate;p-nitro-benzoicaciethylester;RARECHEM AL BI 0193
CAS:	99-77-4
MF:	C9H9NO4
MW:	195.17
EINECS:	202-786-2
Product Categories:	FINE Chemical & INTERMEDIATES;Aromatic Esters;C8 to C9;Carbonyl Compounds;Esters
Mol File:	99-77-4.mol

Ethyl p-nitrobenzoate Chemical Properties

Melting point	55-59 °C (lit.)
Boiling point	182 °C
density	1.3544 (rough estimate)
refractive index	1.5700 (estimate)
storage temp.	2-8°C
solubility	Chloroform (Slightly), Ethyl Acetate (Slightly)
form	Crystalline Powder
color	Yellow
Merck	14,3832
BRN	1912879
CAS DataBase Reference	99-77-4(CAS DataBase Reference)
NIST Chemistry Reference	Ethyl 4-nitrobenzoate(99-77-4)
EPA Substance Registry System	Ethyl 4-nitrobenzoate (99-77-4)

Safety Information

Risk Statements	33
Safety Statements	22-24/25
WGK Germany	3
RTECS	DH5600000
TSCA	Yes
HS Code	29163990

MSDS Information

Provider	Language
SigmaAldrich	English
ACROS	English
ALFA	English

Ethyl p-nitrobenzoate Usage And Synthesis

Chemical Properties	yellow crystalline powder
Uses	Ethyl 4-Nitrobenzoate is used in preparation of p-dimethylaminobenzoate compounds.
General Description	Pharmaceutical secondary standards for application in quality control provide pharma laboratories and manufacturers with a convenient and cost-effective alternative to the preparation of in-house working standards
Purification Methods	Dissolve it in Et2O and wash it with aqueous alkali, then the ether is evaporated and the solid recrystallised from EtOH. [Beilstein 13 H 3787, 13 IV 1074.]

Ethyl p-nitrobenzoate Preparation Products And Raw materials

Raw materials	p-Nitrobenzoic acid
Preparation Products	Benzocaine-->Benzocaine hydrochloride-->Ethyl 4-etoxybenzoate-->Ethyl 4-(butylamino)benzoate-->ISOPROPYL 4-AMINOBENZOATE

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