| 3'-METHOXYPHENACYL BROMIDE Basic information |
| Product Name: | 3'-METHOXYPHENACYL BROMIDE |
| Synonyms: | 3'-Methoxyphenacyl Bromide [for HPLC Labeling];Ethanone, 2-bromo-1-(3-methoxyphenyl)-;bromomethyl 3-methoxyphenyl ketone;AKOS BBS-00003869;ALPHA-BROMO-M-METHOXYACETOPHENONE;ALPHA-BROMO-3'-METHOXYACETOPHENONE;M-METHOXYPHENACYL BROMIDE;2-BROMO-3''-METHOXYACETOPHENONE 97% |
| CAS: | 5000-65-7 |
| MF: | C9H9BrO2 |
| MW: | 229.07 |
| EINECS: | 225-666-1 |
| Product Categories: | Aromatics;Intermediates;Aromatic Halides (substituted);Analytical Chemistry;Carboxyl Group Labeling Reagents for HPLC;HPLC Labeling Reagents;UV Detection (HPLC Labeling Reagents) |
| Mol File: | 5000-65-7.mol |
| 3'-METHOXYPHENACYL BROMIDE Chemical Properties |
| Melting point | 60-62 °C(lit.) |
| Boiling point | 215.8°C (rough estimate) |
| density | 1.4921 (rough estimate) |
| refractive index | 1.5500 (estimate) |
| storage temp. | 2-8°C |
| solubility | soluble in Methanol |
| form | Crystalline Powder |
| color | White to slightly yellow-green |
| BRN | 510128 |
| CAS DataBase Reference | 5000-65-7(CAS DataBase Reference) |
| NIST Chemistry Reference | 2-Bromo-3'-methoxyacetophenone(5000-65-7) |
| Safety Information |
| Hazard Codes | C |
| Risk Statements | 34-36/37-22 |
| Safety Statements | 26-27-28-36/37/39-45-34 |
| RIDADR | UN 3261 8/PG 2 |
| WGK Germany | 3 |
| HazardClass | 8 |
| PackingGroup | III |
| HS Code | 29147000 |
| MSDS Information |
| Provider | Language |
|---|---|
| SigmaAldrich | English |
| ACROS | English |
| ALFA | English |
| 3'-METHOXYPHENACYL BROMIDE Usage And Synthesis |
| Chemical Properties | WHITE TO SLIGHTLY YELLOW-GREEN CRYST. POWDER |
| Uses | Derivatizing reagent. |
| Uses | 2-bromo-3′-methoxyacetophenone, an alkylating agent, has been used to stabilize clopidogrel active metabolite (AM) in human plasma. It has also been used in the derivatisation of active metabolites in blood to ensure its stability during sample processing and storage. |
| Preparation | Obtained by reaction of bromine with 3-methoxyacetophenone in chloroform at 0° for 3 h (88%). |
| 3'-METHOXYPHENACYL BROMIDE Preparation Products And Raw materials |
| Preparation Products | 3-Methoxyacetophenone-->5-(4-(2-(3-METHOXYPHENYL)-2-OXOETHOXY)BENZYL)THIAZOLIDINE-2,4-DIONE-->3-Methoxybenzoylacetonitrile-->2-Bromo-3′-hydroxyacetophenone |
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