| 6-Methoxyisoquinoline Basic information |
| Product Name: | 6-Methoxyisoquinoline |
| Synonyms: | 6-METHOXY-ISOQUINOLINE;6-Methoxyisoquinoline 90%;6-methoxylisoquinoline;6-Methoxy-2-azanaphthalene;Isoquinoline, 6-methoxy-;6-Methoxyisoquinoline ISO 9001：2015 REACH;52986-70-6 |
| CAS: | 52986-70-6 |
| MF: | C10H9NO |
| MW: | 159.18 |
| EINECS: | |
| Product Categories: | blocks;Heterocycles;Quinolines;Heterocyclic Series;Quinoline&Isoquinoline;Aromatics;API intermediates |
| Mol File: | 52986-70-6.mol |
| 6-Methoxyisoquinoline Chemical Properties |
| Boiling point | 88-95?C/0.8 Torr |
| density | 1.130±0.06 g/cm3(Predicted) |
| storage temp. | Sealed in dry,Room Temperature |
| solubility | Chloroform, Dichloromethane |
| form | Oil |
| pka | 6.11±0.10(Predicted) |
| color | Pale Yellow |
| CAS DataBase Reference | 52986-70-6(CAS DataBase Reference) |
| Safety Information |
| Hazard Codes | Xi |
| Hazard Note | Irritant |
| HS Code | 2933499090 |
| MSDS Information |
| 6-Methoxyisoquinoline Usage And Synthesis |
| Chemical Properties | Clear Oil |
| Uses | 6-Methoxy Isoquinoline (cas# 52986-70-6) is a compound useful in organic synthesis. |
| Preparation | 6-Methoxyisoquinoline synthesis: Using benzaldehyde as the starting material, m-methoxybenzaldehyde is obtained through nitration, reduction, diazotization, hydrolysis and methylation, and 3-methoxybenzaldehyde is obtained through condensation with nitromethane Shiff base and reduction of aluminum hydride -p-Phenylethylamine. The Pictet-Spengler reaction of 3-methoxyl-p-phenylethylamine and 40% aqueous formaldehyde produces 6-methoxyl-1,2,3,4-tetrahydroisoquinoline, and then obtains the target compound in dehydrogenation 6-Methoxyisoquinoline. |
| Synthesis Reference(s) | Journal of the American Chemical Society, 69, p. 1939, 1947 DOI: 10.1021/ja01200a028 |
| 6-Methoxyisoquinoline Preparation Products And Raw materials |
| Preparation Products | 6-METHOXY-1,2,3,4-TETRAHYDRO-ISOQUINOLINE |
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