(CYCLOPROPYLMETHYL)TRIPHENYLPHOSPHONIUM BROMIDE

(CYCLOPROPYLMETHYL)TRIPHENYLPHOSPHONIUM BROMIDE
  • CAS No.:14799-82-7
Other grades of this product :
(CYCLOPROPYLMETHYL)TRIPHENYLPHOSPHONIUM BROMIDE Basic information
Product Name:(CYCLOPROPYLMETHYL)TRIPHENYLPHOSPHONIUM BROMIDE
Synonyms:(CYCLOPROPYLMETHYL)TRIPHENYLPHOSPHONIUM BROMIDE;(CYCLOPROPYLMETHYL)TRIPHENYLPHOSPHONIUM BROMIDE, 98+%;cyclopropylmethyl(triphenyl)phosphanium;Phosphonium, (cyclopropylmethyl)triphenyl-, bromide (1:1)
CAS:14799-82-7
MF:C22H22BrP
MW:397.29
EINECS:238-862-7
Product Categories:
Mol File:14799-82-7.mol
(CYCLOPROPYLMETHYL)TRIPHENYLPHOSPHONIUM BROMIDE Chemical Properties
Melting point 182-183°C
storage temp. Inert atmosphere,Room Temperature
Sensitive Hygroscopic
BRN 4068302
CAS DataBase Reference14799-82-7(CAS DataBase Reference)
Safety Information
Risk Statements 36/37/38
Safety Statements 26-36
MSDS Information
ProviderLanguage
ALFA English
(CYCLOPROPYLMETHYL)TRIPHENYLPHOSPHONIUM BROMIDE Usage And Synthesis
SynthesisTriphenylphosphine (3.9 g, 14.8 mmoles) was placed into a 300 mL round bottom flask, equipped with a condenser which was cooled with tap water. Dry benzene (100 mL) (distilled over sodium/benzophenone) was cannulated into the reaction vessel, and a positive pressure of argon and magnetic stirring were maintained throughout the reaction sequence. Cyclopropylmethyl bromide (2.0 g, 14.8 mmoles) was added to the solution via syringe. The reaction mixture was heated at reflux for 10 days producing insoluble cyclopropylmethyltriphenylphosphonium bromide.
(CYCLOPROPYLMETHYL)TRIPHENYLPHOSPHONIUM BROMIDE Preparation Products And Raw materials

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