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| Benzoyl isothiocyanate Basic information |
| Benzoyl isothiocyanate Chemical Properties |
| Melting point | 128 °C | | Boiling point | 128-131 °C/15 mmHg (lit.) | | density | 1.214 g/mL at 25 °C (lit.) | | refractive index | n20/D 1.6354(lit.) | | Fp | >230 °F | | storage temp. | 2-8°C | | solubility | Chloroform | | form | Liquid | | color | Clear yellow to orange-brown | | Specific Gravity | 1.214 | | Water Solubility | almost insoluble | | Sensitive | Moisture Sensitive/Lachrymatory | | Merck | 14,1114 | | BRN | 606716 | | CAS DataBase Reference | 532-55-8(CAS DataBase Reference) | | NIST Chemistry Reference | Benzoyl isothiocyanate(532-55-8) |
| Benzoyl isothiocyanate Usage And Synthesis |
| Chemical Properties | CLEAR YELLOW TO ORANGE-BROWN LIQUID | | Uses | Benzoyl isothiocyanate has been used in the preparation of:- 1-benzoyl-3-(5-chloro-2-hydroxyphenyl)thiourea, new thiourea derivative
- guanine
| | Purification Methods | Distil the isothiocyanate over a small amount of P2O5, whereby the distillate crystallises in prisms. It is readily hydrolysed by H2O to give benzamide and benzoylurea, but with NH3 it gives benzoylurea m 210o which can be recrystallised from EtOH. [Hill & Degnan J Am Chem Soc 62 1595 1940, Terss & McEwen J Am Chem Soc 76 580 1954, Frank & Smith Org Synth Coll Vol III 735 1955, Beilstein 9 IV 777.] |
| Benzoyl isothiocyanate Preparation Products And Raw materials |
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