Other grades of this product :
| Dibenzyl sulphide Basic information |
| Product Name: | Dibenzyl sulphide | | Synonyms: | BENZYLSULFID;BENZYL SULFIDE;DIBENZYL SULFIDE;DIBENZYL SULPHIDE;Benzene, 1,1'-[thiobis(methylene)]bis-;Benzyl sulfide, 98% 100GR;Dibenzyl sulfid;BENZYLSULPHIDE | | CAS: | 538-74-9 | | MF: | C14H14S | | MW: | 214.33 | | EINECS: | 208-703-6 | | Product Categories: | sulfide Flavor | | Mol File: | 538-74-9.mol |
| Dibenzyl sulphide Chemical Properties |
| Dibenzyl sulphide Usage And Synthesis |
| Chemical Properties | beige crystals or powder with an unpleasant smell | | Uses | Organic synthesis. | | Synthesis Reference(s) | Canadian Journal of Chemistry, 53, p. 1480, 1975 DOI: 10.1139/v75-205Tetrahedron Letters, 27, p. 1073, 1986 DOI: 10.1016/S0040-4039(86)80051-X | | General Description | Colorless plates or pale beige crystalline solid with a crippling stench . | | Air & Water Reactions | Insoluble in water. | | Reactivity Profile | Organosulfides, such as Dibenzyl sulphide, are incompatible with acids, diazo and azo compounds, halocarbons, isocyanates, aldehydes, alkali metals, nitrides, hydrides, and other strong reducing agents. Reactions with these materials generate heat and in many cases hydrogen gas. Many of these compounds may liberate hydrogen sulfide upon decomposition or reaction with an acid. | | Fire Hazard | Dibenzyl sulphide is combustible. | | Safety Profile | Moderately toxic by ingestion.When heated to decomposition it emits toxic vapors ofSOx. | | Purification Methods | Crystallise the sulfide from EtOH/water (10:1), or repeatedly from Et2O. It has also been purified by chromatography on Al2O3 (pentane as eluent), then recrystallised from EtOH [Kice & Bowers J Am Chem Soc 84 2390 1962]. Dry it in a vacuum at 30o over P2O5, fused under nitrogen and re-dried. [Beilstein 6 IV 2649.] |
| Dibenzyl sulphide Preparation Products And Raw materials |
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