1,6-Diisopropyl-3,8-dibromopyrene

1,6-Diisopropyl-3,8-dibromopyrene
  • CAS No.:869340-02-3
Other grades of this product :
1,6-Diisopropyl-3,8-dibromopyrene Basic information
Product Name:1,6-Diisopropyl-3,8-dibromopyrene
Synonyms:1,6-Diisopropyl-3,8-dibromopyrene;1,6-dibromo-3,8-diisopropylpyrene;Pyrene,1,6-dibromo -3,8-bis(1-methylethyl)-
CAS:869340-02-3
MF:C22H20Br2
MW:444.2
EINECS:
Product Categories:
Mol File:869340-02-3.mol
1,6-Diisopropyl-3,8-dibromopyrene Chemical Properties
Boiling point 512.4±45.0 °C(Predicted)
density 1.508±0.06 g/cm3 (20 ºC 760 Torr)
storage temp. Keep in dark place,Sealed in dry,Room Temperature
form powder to crystal
color White to Orange to Green
Safety Information
MSDS Information
1,6-Diisopropyl-3,8-dibromopyrene Usage And Synthesis
Uses1,6-Diisopropyl-3,8-dibromopyrene can be used as organic synthesis intermediates and pharmaceutical intermediates, mainly used in laboratory research and development processes and chemical production processes.
SynthesisIn a three-neck round bottom flask, dissolve 2.86 g (10 mmol) of Intermediate-1 in 40 mL of CCl4. Dropped in a round bottom flask 4.00 g (25 mol) of Br 2 and 30 mL of CCl 4 were added to the funnel, and the mixture was slowly dropped into a round bottom flask over 4 hours N2 is injected to remove HBr generated. When dropping is completed, stirring is carried out under N2 air flow for 1 hour When the reaction was terminated, the resulting precipitate was filtered as it was, and the precipitate was recrystallized using toluene to give (2.8 g, 58%).
1,6-Diisopropyl-3,8-dibromopyrene Preparation Products And Raw materials

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