Iodoacetonitrile

CAS No.：624-75-9

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This product is a chemical product/pharmaceutical intermediate. It is not a drug, an active pharmaceutical ingredient (API), or a pharmaceutical-grade material. It has not been granted a drug approval number or a Chemical Drug Substance Approval Notice, has not passed drug-related review and approval, and is not manufactured, tested, or released in accordance with pharmaceutical GMP.
This product is intended solely for non-clinical research, process development, quality studies, further chemical processing, or chemical synthesis. It must not be used in drug-product manufacturing, clinical trials, clinical diagnosis, or administration to humans or animals, or be sold, used as an input, submitted for regulatory filing, or released as an API or pharmaceutical material.
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Iodoacetonitrile Basic information

Product Name:	Iodoacetonitrile
Synonyms:	Acetonitrile, iodo-;AKOS 91685;Iodoacetonitrile,97%;IODOACETONITRILE;iodomethyl cyanide;10doacetonitrile;2-Iodoacetonitrile;Cyanoiodomethane
CAS:	624-75-9
MF:	C2H2IN
MW:	166.95
EINECS:	210-860-0
Product Categories:	C1 to C5;Cyanides/Nitriles;Nitrogen Compounds
Mol File:	624-75-9.mol

Iodoacetonitrile Chemical Properties

Boiling point	182-184 °C/720 mmHg (lit.)
density	2.307 g/mL at 25 °C (lit.)
refractive index	n20/D 1.574(lit.)
RTECS	AM0740000
Fp	187 °F
storage temp.	2-8°C
form	Liquid
Specific Gravity	2.307
color	Clear red to brown
Water Solubility	Soluble in benzene, alcohol, acetone, ether. Slightly soluble in water. Insoluble in hexane.
Sensitive	Light Sensitive
BRN	1734628
Exposure limits	NIOSH: IDLH 25 mg/m3
CAS DataBase Reference	624-75-9(CAS DataBase Reference)
NIST Chemistry Reference	Iodoacetonitrile(624-75-9)
EPA Substance Registry System	Acetonitrile, iodo- (624-75-9)

Safety Information

Hazard Codes	C,T
Risk Statements	22-34-36/37/38-23/24/25
Safety Statements	26-36/37/39-45-24/25
RIDADR	UN 3265 8/PG 2
WGK Germany	3
F	8-10-19-21
HazardClass	8
PackingGroup	II
HS Code	29269090

MSDS Information

Provider	Language
Iodoacetonitrile	English
ACROS	English
SigmaAldrich	English
ALFA	English

Iodoacetonitrile Usage And Synthesis

Chemical Properties	clear red to brown liquid
Uses	Iodoacetonitrile is used for alkylation of nucleophiles. It undergoes Reformatsky and Wittig-type reactions with aldehydes.

Iodoacetonitrile Preparation Products And Raw materials

Raw materials

2-(MethylphenylaMino)-acetonitrile-->2-(ethyl(phenyl)aMino)acetonitrile-->[methyl(phenyl)amino]acetonitrile-->Benzenaminium,N-ethyl-N,N-dimethyl-, iodide (1:1)-->2,4-Difluoroiodobenzene-->N-ETHYL-N-METHYLANILINE-->Phenyltrimethylammonium iodide-->2,6-Difluoroiodobenzene-->Chloroacetonitrile-->Acetonitrile-->Iodomethane-->Cyanoacetic acid

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