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| 1,4-Dibromopentane Basic information |
| Product Name: | 1,4-Dibromopentane | | Synonyms: | sodium 1-amino-4-(2,4-dimethylanilino)-9,10-dioxo-2-anthracenesulfonate;1,4-DibroMopentane, 97% 25GR;1,4-DIBROMOPENTANE;(RS)-1,4-Dibromopentane;1,4-dibromo-pentan;1,4-DibromopentaneDISC 05/09/02;pentane,1,4-dibromo-;1,4-Dibromopentane,97% | | CAS: | 626-87-9 | | MF: | C5H10Br2 | | MW: | 229.94 | | EINECS: | 210-967-2 | | Product Categories: | Alkyl;Halogenated Hydrocarbons;Organic Building Blocks | | Mol File: | 626-87-9.mol |
| 1,4-Dibromopentane Chemical Properties |
| 1,4-Dibromopentane Usage And Synthesis |
| Chemical Properties | clear colorless to light yellow-brown liquid with a wine smell. | | Uses | 1,4-Dibromopentane is used in the preparation of pharaoh ant trail pheromone stereoisomer, indolizidine alkaloid. It is also involved in the preparation 1,2-dimethyl-1-phenylcyclopentane and boc-L-2-amino-6-bromoheptanoic acid. | | Preparation | 1,4-Dibromopentane is synthesized by ring-opening bromination of 2-methyltetrahydrofuran with hydrobromic acid and sulfuric acid. First, add hydrobromic acid into the reaction pot for cooling, slowly add 2-methyltetrahydrofuran and sulfuric acid in turn under stirring, and finish the addition when the temperature does not exceed 40°C. The temperature was raised to 60°C, reacted for 2h, and then reacted at 80-85°C for 4h. After cooling, the bromide was separated and washed with water until neutral to obtain 1,4-dibromopentane as an oily substance. Yield 92.5%. | | Synthesis Reference(s) | Journal of the American Chemical Society, 74, p. 917, 1952 DOI: 10.1021/ja01124a016 |
| 1,4-Dibromopentane Preparation Products And Raw materials |
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