| METHYL 4-(BROMOMETHYL)-3-METHOXYBENZOATE Basic information |
| Preparation |
| Product Name: | METHYL 4-(BROMOMETHYL)-3-METHOXYBENZOATE |
| Synonyms: | Methyl 4-(bromomethyl)-3-methoxybenzonate;4-BROMOMETHYL-3-METHOXY-BENZOIC ACID METHYL ESTER;METHYL3-METHOXY-4-(BROMOMETHYL)BENZONATE;METHYL4-BROMOETHYL-3-METHOXYBENZOATE;4-Brommethyl-3-methoxybenzoesuremethylester;Methyl 4-brome methyl-3-methoxy benzoate;Methyl 4-(bromomethyl)-3-(methyloxy)benzoate;Methyl 4-(bromomethyl)-3-methoxybenzoate 98% |
| CAS: | 70264-94-7 |
| MF: | C10H11BrO3 |
| MW: | 259.1 |
| EINECS: | 410-310-1 |
| Product Categories: | Building Blocks;C10 to C11;Aromatic Esters;Carbonyl Compounds;Chemical Synthesis;Organic Building Blocks;Benzoic acid;C10 to C11;Carbonyl Compounds;Esters |
| Mol File: | 70264-94-7.mol |
| METHYL 4-(BROMOMETHYL)-3-METHOXYBENZOATE Chemical Properties |
| Melting point | 92-94°C |
| Boiling point | 324.2±32.0 °C(Predicted) |
| density | 1.432 |
| storage temp. | under inert gas (nitrogen or Argon) at 2-8°C |
| form | powder to crystal |
| color | White to Light yellow |
| CAS DataBase Reference | 70264-94-7(CAS DataBase Reference) |
| Safety Information |
| Hazard Codes | Xi,N |
| Risk Statements | 36/37/38-50/53-43-41-38 |
| Safety Statements | 26-36/37/39-61-60 |
| RIDADR | UN 2811 6.1/PG 3 |
| WGK Germany | 3 |
| HazardClass | IRRITANT |
| PackingGroup | Ⅲ |
| HS Code | 2918999090 |
| MSDS Information |
| METHYL 4-(BROMOMETHYL)-3-METHOXYBENZOATE Usage And Synthesis |
| Preparation | Methyl 4-(bromomethyl)-3-methoxybenzoate is prepared by the following steps:A mixture of methyl 3-methoxy-4-methylbenzoate 37 (5 g, 27.8 mmol), NBS (4.94 g, 27.8 mmol), and benoyl peroxide (0.0008 g, 0.003 mmol) was refluxed in CCl4 (25 ml) for 10 hours. The reaction mixture was allowed to cool and filtered. The residue was washed with CCl4 and the combined filtrate concentrated in vacuo. Purification by column chromatography over silica gel (5-10% EtOAc-pet ether) furnished a colourless solid (7.19 g).Yield : 100% |
| METHYL 4-(BROMOMETHYL)-3-METHOXYBENZOATE Preparation Products And Raw materials |
| Raw materials | Dimethyl sulfate-->Carbon tetrachloride-->N-Bromosuccinimide-->2,2'-Azobis(2-methylpropionitrile)-->3-Hydroxy-4-methylbenzoic acid |
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