Product

1-Chloro-N,N,2-trimethylpropenylamine

CAS No.：26189-59-3

Other grades of this product :

1-Chloro-N,N,2-trimethylpropenylamine Basic information

Product Name:	1-Chloro-N,N,2-trimethylpropenylamine
Synonyms:	TETRAMETHYL-ALPHA-CHLORENAMINE;1-CHLORO-N,N,2-TRIMETHYL-1-PROPENYLAMINE;1-CHLORO-N,N,2-TRIMETHYLPROPENYLAMINE;(1-CHLORO-2-METHYLPROPENYL)DIMETHYLAMINE;1-Chloro-N,N,2-trimethylpropenylamine, 98.5+%;1-Chloro-N,N,2-trimethylpropenylamine ,98%;Ghosez′s reagent;1-Chloro-N,N,2-triMethylpropenylaMine, 98.5+% 5ML
CAS:	26189-59-3
MF:	C6H12ClN
MW:	133.62
EINECS:
Product Categories:	Alkenyl;Halogenated Hydrocarbons;Organic Building Blocks
Mol File:	26189-59-3.mol

1-Chloro-N,N,2-trimethylpropenylamine Chemical Properties

Boiling point	129-130 °C(lit.)
density	1.01 g/mL at 25 °C(lit.)
refractive index	n20/D 1.453(lit.)
Fp	80 °F
storage temp.	2-8°C
solubility	Chloroform (Sparingly), Methanol (Slightly)
form	Liquid
pka	4.27±0.70(Predicted)
color	Colorless to yellow
Stability:	Hygroscopic, Moisture Sensitive, Unstable in Solution

Safety Information

Hazard Codes	C
Risk Statements	10-34
Safety Statements	16-26-36/37/39-45
RIDADR	UN 2734 8/PG 1
WGK Germany	3
HS Code	29211990

MSDS Information

Provider	Language
ACROS	English
SigmaAldrich	English

1-Chloro-N,N,2-trimethylpropenylamine Usage And Synthesis

Chemical Properties	Colorless to yellow liquid
Uses	1-Chloro-N,N,2-trimethyl-1-propenylamine is an acid halogenation reagent developed by Ghosez, that enables the conversion of carboxylic acids into the corresponding chlorides under strictly neutral conditions. This method was successfully used in the total synthesis of caloporoside, roseophilin, (-)-enniatin B, (±)-epimeloscine and (±)-meloscine.
Synthesis Reference(s)	Journal of the American Chemical Society, 94, p. 2869, 1972 DOI: 10.1021/ja00763a061Organic Syntheses, Coll. Vol. 6, p. 282, 1988Tetrahedron Letters, 25, p. 5043, 1984 DOI: 10.1016/S0040-4039(01)91114-1

1-Chloro-N,N,2-trimethylpropenylamine Preparation Products And Raw materials

Raw materials

Dichloromethane-->N,N-Dimethylformamide-->PETROLEUM ETHER-->Phosphorus oxychloride-->Magnesium sulfate-->Triethylamine-->Sodium bicarbonate-->Dimethylamine-->Isobutyryl chloride

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