IODOMETHANE-D3

IODOMETHANE-D3
  • CAS No.:865-50-9
Other grades of this product :
IODOMETHANE-D3 Basic information
Product Name:IODOMETHANE-D3
Synonyms:Deuterated iodomethane;N,N-dimethylaniline-methyl--D6;Trideuteromethyl iodide;Perdeuteriomethyl iodide;Perdeuteroiodomethane;Trideuterioiodomethane;Iodomethane-d3 99 atom % D;IODOMETHANE-D3
CAS:865-50-9
MF:CD3I
MW:144.96
EINECS:212-744-5
Product Categories:
Mol File:865-50-9.mol
IODOMETHANE-D3 Chemical Properties
Melting point -66.5 °C(lit.)
Boiling point 42 °C(lit.)
density 2.330 g/mL at 25 °C
vapor density 4.89 (vs air)
vapor pressure 22.83 psi ( 55 °C)
refractive index n20/D 1.5262(lit.)
storage temp. 0-6°C
solubility Chloroform, Methanol (Slightly)
form Liquid
color Clear colorless
BRN 1732026
Stability:Stable. Incompatible with strong bases, strong oxidizing agents. Moisture and light-sensitive.
InChIKeyINQOMBQAUSQDDS-FIBGUPNXSA-N
EPA Substance Registry SystemMethane-d3, iodo- (865-50-9)
Safety Information
Hazard Codes T
Risk Statements 21-23/25-34-40-42/43-37/38-53
Safety Statements 26-36/37/39-38-45-36/37
RIDADR UN 2644 6.1/PG 1
WGK Germany 3
8-10-21
HazardClass 6.1(a)
PackingGroup I
HS Code 28459010
MSDS Information
ProviderLanguage
SigmaAldrich English
ACROS English
IODOMETHANE-D3 Usage And Synthesis
DescriptionA deuterated form of iodomethane made from methanol-D4.IODOMETHANE-D3 is an important component in the organic synthesis of deuterium-labeled compounds.
Chemical PropertiesIODOMETHANE-D3 is a colorless liquid, sensitive to light and volatile.
UsesIODOMETHANE-D3 can be used as a methylating agent in organic synthesis.
UsesIODOMETHANE-D3 is used in the analysis of peptides and glycans using various analytical spectroscopic techniques.
SynthesisAn efficient method for the preparation of IODOMETHANE-D3, using METHANOL-D3 and iodine monomers as reaction materials, in a hydrogen atmosphere, with the addition of transition metal catalysts and ligands to produce IODOMETHANE-D3 in situ at 0°C-120°C.
IODOMETHANE-D3 Preparation Products And Raw materials
Raw materialsmethyl-d3 radical-->METHANOL-D3-->METHYL-D3 P-TOLUENESULFONATE-->BROMOMETHANE-D3-->Methanol-d4
Preparation ProductsMETHYL-D3-MAGNESIUM IODIDE-->N-METHYL-D3-PIPERAZINE

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