4-Diazodiphenylamine sulfate

4-Diazodiphenylamine sulfate
  • CAS No.:4477-28-5
Other grades of this product :
4-Diazodiphenylamine sulfate Basic information
Product Name:4-Diazodiphenylamine sulfate
Synonyms:4-(phenylamino)-benzenediazoniusulfate(1:1);AcnaBlueRTSalt;BluebaseRT;BlueSaltNR;C.I.AzoicDiazoComponent22(37240);DaitoBlueSaltVR;FastbluesaltVRT;FastBlueVRTSalt
CAS:4477-28-5
MF:C12H11N3O4S
MW:293.3
EINECS:224-756-8
Product Categories:Photosensitizer for Negative PR;Dyes and Pigments
Mol File:4477-28-5.mol
4-Diazodiphenylamine sulfate Chemical Properties
Boiling point 623.17℃[at 101 325 Pa]
density 1.512[at 20℃]
vapor pressure 0Pa at 25℃
Colour Index 37240
Water Solubility 21.24g/L at 20℃
LogP1.28 at 23℃
CAS DataBase Reference4477-28-5(CAS DataBase Reference)
EPA Substance Registry SystemBenzenediazonium, 4-(phenylamino)-, sulfate (1:1) (4477-28-5)
Safety Information
WGK Germany 3
MSDS Information
ProviderLanguage
SigmaAldrich English
4-Diazodiphenylamine sulfate Usage And Synthesis
Flammability and ExplosibilityNotclassified
Purification MethodsDissolve 10g of the dye in 100mL of hot water. Sodium dithionite (0.4g) is then added, followed by active carbon (1.5g) and is filtered hot. To the colourless or slightly yellow filtrate a solution of saturated NaCl is added, and the mixture is cooled. The needles are filtered off, washed with cold water, dried at room temperature, and stored in a dark bottle (light sensitive). [Anderson & Steedly J Am Chem Soc 76 5144 1954, Erdey Chem Analyst 48 106 1959, Beilstein 16 H 602, 16 I 371, 16 II 307, 16 III 575. ]
4-Diazodiphenylamine sulfate Preparation Products And Raw materials
Raw materialsSodium nitrite-->Sodium sulfide-->4-Chloronitrobenzene-->Diphenylamine-->4-Aminodiphenylamine-->4-NITROSODIPHENYLAMINE

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