1,4-Bis-[4-(3-acryloyloxypropyloxy)benzoyloxy]-2-methylbenzene

1,4-Bis-[4-(3-acryloyloxypropyloxy)benzoyloxy]-2-methylbenzene
  • CAS No.:174063-87-7

Important Notice

  1. This product is a chemical product/pharmaceutical intermediate. It is not a drug, an active pharmaceutical ingredient (API), or a pharmaceutical-grade material. It has not been granted a drug approval number or a Chemical Drug Substance Approval Notice, has not passed drug-related review and approval, and is not manufactured, tested, or released in accordance with pharmaceutical GMP.
  2. This product is intended solely for non-clinical research, process development, quality studies, further chemical processing, or chemical synthesis. It must not be used in drug-product manufacturing, clinical trials, clinical diagnosis, or administration to humans or animals, or be sold, used as an input, submitted for regulatory filing, or released as an API or pharmaceutical material.
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1,4-Bis-[4-(3-acryloyloxypropyloxy)benzoyloxy]-2-methylbenzene Basic information
Product Name:1,4-Bis-[4-(3-acryloyloxypropyloxy)benzoyloxy]-2-methylbenzene
Synonyms:1,4-Bis-[4-(3-acryloyloxypropyloxy)benzoyloxy]-2-Methylbenzene 4-(3-Acryloyloxypropyloxy)-benzoesure -2-Methyl-1, 4-phenylester;2-Methyl-1,4-phenylene-bis[4[3(acryloyloxy)propyloxy]benzoate];4-(3-Acryloyloxypropyloxy)benzoic acid 2-methyl-1,4-phenylene ester;2-Methyl-1,4-phenylene bis(4-(3-(acryloyloxy)propoxy)benzoate);Benzoic acid, 4-[3-[(1-oxo-2-propenyl)oxy]propoxy]-,2-methyl-1,4-phenylene ester;4- (3-acryloyloxy-propoxy) benzoic acid 2-methyl-1,4-phenylene ester;1,4-Bis-[4-(3-acryloyloxypropyloxy)benzoyloxy]-2-methylbenze;4-(3-Acryloyloxypropyloxy)-benzoesure 2-methyl-1, 4-phenylester
CAS:174063-87-7
MF:C33H32O10
MW:588.6
EINECS:425-560-7
Product Categories:
Mol File:174063-87-7.mol
1,4-Bis-[4-(3-acryloyloxypropyloxy)benzoyloxy]-2-methylbenzene Chemical Properties
Boiling point 733.5±60.0 °C(Predicted)
density 1.219
vapor pressure 0.003Pa at 25℃
storage temp. Keep in dark place,Sealed in dry,Room Temperature
Water Solubility 5.3μg/L at 20℃
LogP5.3 at 40℃
Safety Information
HS Code 2917399590
MSDS Information
1,4-Bis-[4-(3-acryloyloxypropyloxy)benzoyloxy]-2-methylbenzene Usage And Synthesis
Chemical PropertiesWhite to Almost white powder to crystal
Application1,4-Bis-[4-(3-acryloyloxypropyloxy)benzoyloxy]-2-methylbenzene is one of numerous organic compounds composing American Elements's comprehensive catalog of life science products.
Flammability and ExplosibilityNotclassified
SynthesisThe synthesis of 1,4-Bis-[4-(3-acryloyloxypropyloxy)benzoyloxy]-2-methylbenzene is as follows:Stirrer, was added methanesulfonyl chloride 5.00 g (43.6 mmol) and tetrahydrofuran 10mL the reactor having a thermometer and two dropping device. Ice-cold while each by dropping a tetrahydrofuran solution 30mL of formula tetrahydrofuran solution 60mL and triethylamine 5.25g of (I-3-1) represented by the compound 12.9g (44.1 mmol) of (51.9 mmol) from device (equation (solution of the compound represented by I-3-1)) :( triethylamine solution) = 2: were added dropwise simultaneously with one of the drip rate.After stirring for 1 hour while cooling with ice, it was added 4-dimethylaminopyridine 2.64 g (21.6 mmol) and 2- (4-hydroxyphenyl) ethanol 2.69 g (19.4 mmol).With ice-cooling was added dropwise triethylamine 5.25g (51.9 mmol).After stirring for 7 hours, the solvent was distilled off and treated added for liquid separation dichloromethane and 5% hydrochloric acid.After the organic layer was washed with brine neutralization, and purified by column chromatography (silica gel) and reprecipitated (dichloromethane / methanol) to give the compound 12.2g of formula (I-3).82% yield, had a purity of 99.63%.
1,4-Bis-[4-(3-acryloyloxypropyloxy)benzoyloxy]-2-methylbenzene Preparation Products And Raw materials
Raw materials4-(3-ACRYLOYLOXY-N-PROP-1-YLOXY)BENZOIC ACID-->2-Methylhydroquinone

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