Other grades of this product :
| 3'-Hydroxypropiophenone Basic information |
| Product Name: | 3'-Hydroxypropiophenone | | Synonyms: | 1-(3-hydroxyphenyl)propan-1-one;1-Propanone,1-(3-hydroxyphenyl)-;3-HYDROXY PROPIOPHENONE;3'-HYDROXYPROPIOPHENONE;Metaraminol Bitartrate Impurity 13 | | CAS: | 13103-80-5 | | MF: | C9H10O2 | | MW: | 150.17 | | EINECS: | 236-027-1 | | Product Categories: | | Mol File: | 13103-80-5.mol |
| 3'-Hydroxypropiophenone Chemical Properties |
| Melting point | 82 °C | | Boiling point | 288.9±23.0 °C(Predicted) | | density | 1.104±0.06 g/cm3(Predicted) | | storage temp. | Inert atmosphere,Room Temperature | | pka | 9.09±0.10(Predicted) | | CAS DataBase Reference | 13103-80-5(CAS DataBase Reference) |
| 3'-Hydroxypropiophenone Usage And Synthesis |
| Uses | 1-?(3-?Hydroxyphenyl)?-?1-?propanone is a reactant used to synthesize tricyclic fused pyridines, a family of alkaloids with antimalarial activity. | | Preparation | Preparation by diazotization of m-aminopropiophenone, followed by decomposition of the diazonium salt obtained, (71%) Also obtained by saponification of 3-acetoxypropiophenone (b.p.2 127–128°) with refluxing 10% sodium hydroxide for 2–3 h (83%) Also obtained by reductive deamination of 2-amino-5-hydroxypropiophenone (diazotization, followed by decomposition of the diazonium salt formed with copper powder in ethanol) Also obtained by reaction of ethylmagnesium bromide with 3-hydroxy-N, N-diethylbenzamide in refluxing n-butyl ether for 4 h (75%) Also obtained by treatment of 3-methoxypropiophenone (b.p.0.05 70–76°) with pyridinium chloride at 210° for 30 min (85%) Also obtained by treatment of 1-hydroxy-1-(3-hydroxyphenyl)propane (m.p. 105–107°) with DDQ in dioxane for 72 h (97%). |
| 3'-Hydroxypropiophenone Preparation Products And Raw materials |
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