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| 5-Bromothiazole Basic information |
| 5-Bromothiazole Chemical Properties |
| Melting point | 131-132 °C(Solv: ligroine (8032-32-4)) | | Boiling point | 80-81°C/18mm | | density | 1.835 at 25 °C | | refractive index | 1.5955 | | Fp | 170°F | | pka | 1.00±0.10(Predicted) | | form | Liquid | | color | Clear yellow to brown | | Water Solubility | Soluble in water. | | Sensitive | Moisture Sensitive | | CAS DataBase Reference | 3034-55-7(CAS DataBase Reference) |
| 5-Bromothiazole Usage And Synthesis |
| Uses | 5-Bromothiazole is used as a pharmaceutical intermediate and performance material. | | General Description | 5-Bromothiazole is a monobromothiazole, which can be prepared via treatment of 2,5-dibromothiazole with sodium ethoxide followed by hydrogenation over spongy nickel. | | Purification Methods | If bromothiazole is too coloured, then suspend it in dilute NaOH and steam distil it. Add NaCl to the aqueous distillate, extract it with Et2O, dry it (Na2SO4), evaporate and fractionate the residue in a vacuum. The HgCl2 salt crystallises from EtOH with m 148o (dec). [Beyerman et al. Recl Trav Chim, Pays Bas 73 330 1954, Beilstein 27 III/IV 962.] |
| 5-Bromothiazole Preparation Products And Raw materials |
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