Product

N-(9-Fluorenylmethoxycarbonyloxy)succinimide

CAS No.：82911-69-1

Other grades of this product :

N-(9-Fluorenylmethoxycarbonyloxy)succinimide Basic information

Product Name:	N-(9-Fluorenylmethoxycarbonyloxy)succinimide
Synonyms:	1-[[(9h-fluoren-9-ylmethoxy)carbonyl]oxy]-5-pyrrolidinedione;9-fluorenylmethoxycarbonyloxysuccinimide;9-fluorenylmethyl-n-succinimide carbonate;N-(9-FluorenylmethoxyCarbonyloxy)Succinimide9-Fluorenylmethylsuccinimidylcarbonate;CARBONIC ACID 2,5-DIOXO-PYRROLIDIN-1-YL ESTER 9H-FLUOREN-9-YLMETHYL ESTER;CARBONIC ACID FLUORENYLMETHYL SUCCIN-N-YL-ESTER;FMOC-OSU;FMOC-ONSU
CAS:	82911-69-1
MF:	C19H15NO5
MW:	337.33
EINECS:	433-520-5
Product Categories:	Fmoc-OSU;peptides;Medical Intermediates;Benzocycles;Fluorenes, Flurenones;Pyrrolidines;Amino Acid Derivatives;N-Protecting Reagents;Biochemistry;Condensation & Active Esterification;Fluorenes;Fluorenes & Fluorenones;Heterocycles;Miscellaneous Reagents;N-Substituted Maleimides, Succinimides & Phthalimides;N-Substituted Succinimides;Peptide Synthesis;Protective Reagents (Peptide Synthesis);Synthetic Organic Chemistry;Fmoc-Amino acid series;bc0001
Mol File:	82911-69-1.mol

N-(9-Fluorenylmethoxycarbonyloxy)succinimide Chemical Properties

Melting point	150-153 °C(lit.)
Boiling point	150-153°C
density	1.3460 (rough estimate)
refractive index	1.5000 (estimate)
storage temp.	2-8°C
solubility	Soluble in dimethyl sulfoxide and dimethyl formamide.
form	Microfine Powder
color	White or almost white
Sensitive	Moisture Sensitive
BRN	3569540
CAS DataBase Reference	82911-69-1(CAS DataBase Reference)

Safety Information

Hazard Codes	Xi,N,Xn
Risk Statements	36/37/38-51/53-43-22
Safety Statements	22-24/25-26/37/39-26-61-37-24
RIDADR	UN 3077 9 / PGIII
WGK Germany	3
F	10-21
Hazard Note	Moisture Sensitive
HazardClass	9
HS Code	29251995

MSDS Information

Provider	Language
SigmaAldrich	English
ACROS	English
ALFA	English

N-(9-Fluorenylmethoxycarbonyloxy)succinimide Usage And Synthesis

Chemical Properties	White powder
Uses	N-(9-Fluorenylmethoxycarbonyloxy)succinimide is used in conjunction with Isothiocyanate to conduct partial Edman Degradation on biologically active peptides.
Uses	N-protecting reagent for oligonucleotide and peptide syntheses
Uses	Reagent for the preparation of pure Fmoc amino acids free from contamination by Fmoc-dipeptides.
Purification Methods	Recrystallise the carbonate from CHCl3/Et2O, or from pet ether (b 40-60o). [Pauet Can J Chem 60 976 1982, Lapatsaris et al. Synthesis 671 1983.]

N-(9-Fluorenylmethoxycarbonyloxy)succinimide Preparation Products And Raw materials

Preparation Products

[2-[2-(Fmoc-amino)ethoxy]ethoxy]acetic acid-->FMOC-L-PROPARGYLGLYCINE-->FMOC-b-Ala-OH-->FMOC-L-Leucine-->FMOC-D-PHG-OH-->Fmoc-L-4-Iodophenylalanine-->Fmoc-4-nitro-L-phenylalanine-->FMOC-L-Arginine-->Fmoc-Cys(tBu)-OH-->N-Boc-N'-Fmoc-L-Lysine-->Fmoc-L-hydroxyproline-->FMOC-(2S,3R)-2-AMINO-3-HYDROXY-4-METHYLPENTANOIC ACID-->Piperidine, 1-(9H-fluoren-9-ylmethyl)--->FMOC-2-(2-AMINOETHOXY)ETHANOL-->N-Fmoc-L-homoserine-->Nalpha-FMOC-L-Tryptophan-->FMOC-L-Methionine

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