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| N-BOC-6-METHOXYINDOLE Basic information | | Synthesis |
| Product Name: | N-BOC-6-METHOXYINDOLE | | Synonyms: | TERT-BUTYL 6-HYDROXY-1H-INDOLE-1-CARBOXYLATE;1H-Indole-1-carboxylicacid,6-hydroxy-,1,1-diMethylethylester;6-Hydroxyindole, N-BOC protected 95%;tert-butyl 6-hydroxyindole-1-carboxylate | | CAS: | 898746-82-2 | | MF: | C13H15NO3 | | MW: | 233.26 | | EINECS: | | Product Categories: | | Mol File: | 898746-82-2.mol |
| N-BOC-6-METHOXYINDOLE Chemical Properties |
| Boiling point | 374.5±34.0 °C(Predicted) | | density | 1.16±0.1 g/cm3(Predicted) | | storage temp. | 2-8°C | | pka | 9.48±0.40(Predicted) |
| N-BOC-6-METHOXYINDOLE Usage And Synthesis |
| Synthesis | Tert-butyl 6-fluoro-5-hydroxy-1H-indazole-1-carboxylate was prepared as
described for intermediate tert-butyl 5-hydroxy-1H-indazole-1-carboxylate/ tert-butyl 5-hydroxy-2H-indazole-2-
carboxylate replacing tert-butyl 5-((tert-butyldimethylsilyl)oxy)-1H-indazole-1-carboxylate / tert-butyl 5-((tertbutyldimethylsilyl)
oxy)-2H-indazole-2-carboxylate with tert-butyl 5-((tert-butyldimethylsilyl)oxy)-6-fluoro-1H-indazole-1-carboxylate(yield: 94%). 1H
NMR (400 MHz, Chloroform-d) δ 8.06 (d, J = 0.9 Hz, 1H), 7.95 (d, J = 10.7 Hz, 1H), 7.28 (d, J
= 8.2 Hz, 2H), 5.48 (s, 1H), 1.71 (s, 9H). |
| N-BOC-6-METHOXYINDOLE Preparation Products And Raw materials |
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