3,5-Dinitrobenzoyl chloride

3,5-Dinitrobenzoyl chloride
  • CAS No.:99-33-2
Other grades of this product :
3,5-Dinitrobenzoyl chloride Basic information
Product Name:3,5-Dinitrobenzoyl chloride
Synonyms:3,5-Dinitrobenzoicchloride;3,5-dinitrobenzoyl;3,5-dinitro-benzoylchlorid;DNBC;3,5-DINITROBENZOYL CHLORIDE;3,5-dinitrobenzoic acid chloride;3,4-DINITROBENZOYL CHLORIDE;3,5-DINITROBENZOYL CHLORIDE, FOR FLUORES CENCE
CAS:99-33-2
MF:C7H3ClN2O5
MW:230.56
EINECS:202-750-6
Product Categories:API intermediates;Amino Group Labeling Reagents for HPLC;Hydroxyl Group Labeling Reagents for HPLC;Analytical Chemistry;HPLC Labeling Reagents;UV Detection (HPLC Labeling Reagents)
Mol File:99-33-2.mol
3,5-Dinitrobenzoyl chloride Chemical Properties
Melting point 68-69 °C(lit.)
Boiling point 196 °C11 mm Hg(lit.)
density 1.8836 (rough estimate)
vapor density 7.6 (vs air)
refractive index 1.6290 (estimate)
Fp 196°C/12mm
storage temp. 2-8°C
form Crystals or Crystalline Needles
color Yellow to beige
Water Solubility Slightly soluble in water.
Sensitive Moisture Sensitive
Merck 14,3277
BRN 990249
Stability:Stable. Incompatible with strong oxidizing agents, water, moisture, nitrates, combustible material. Refrigerate.
CAS DataBase Reference99-33-2(CAS DataBase Reference)
NIST Chemistry ReferenceBenzoyl chloride, 3,5-dinitro-(99-33-2)
EPA Substance Registry SystemBenzoyl chloride, 3,5-dinitro- (99-33-2)
Safety Information
Hazard Codes C
Risk Statements 34
Safety Statements 26-36/37/39-45-25
RIDADR UN 3261 8/PG 2
WGK Germany 3
RTECS DM6637000
21
Hazard Note Corrosive
TSCA Yes
HazardClass 8
PackingGroup II
HS Code 29163900
HS Code 29400090
MSDS Information
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3,5-Dinitrobenzoyl chloride English
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ACROS English
ALFA English
3,5-Dinitrobenzoyl chloride Usage And Synthesis
Chemical Propertiesyellow-brown solid
Uses3,5-dinitrobenzoyl chloride is an important intermediate for organic synthesis.
UsesUsed in photography. This aromatic compound is used by chemists to identify alcohol components in esters and in the fluorometric analysis of creatinine.
Purification MethodsCrystallise it from CCl4 or pet ether (b 40-60o). It reacts readily with H2O and should be kept in sealed ampoules. [Beilstein 9 IV 1350.]
3,5-Dinitrobenzoyl chloride Preparation Products And Raw materials
Raw materialsThionyl chloride-->Carbon tetrachloride-->3,5-Dinitrobenzoic acid
Preparation Products(+)-DISPARLURE-->Vitamin D2-->SAPERCONAZOLE-->3,5-DINITROBENZALDEHYDE-->(S)-(+)-N-(3,5-DINITROBENZOYL)-ALPHA-PHENYLGLYCINE

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