3,5-Dinitrobenzoyl chloride

CAS No.：99-33-2

Important Notice

This product is a chemical product/pharmaceutical intermediate. It is not a drug, an active pharmaceutical ingredient (API), or a pharmaceutical-grade material. It has not been granted a drug approval number or a Chemical Drug Substance Approval Notice, has not passed drug-related review and approval, and is not manufactured, tested, or released in accordance with pharmaceutical GMP.
This product is intended solely for non-clinical research, process development, quality studies, further chemical processing, or chemical synthesis. It must not be used in drug-product manufacturing, clinical trials, clinical diagnosis, or administration to humans or animals, or be sold, used as an input, submitted for regulatory filing, or released as an API or pharmaceutical material.
The purchaser must not use this product, or supply it to another party, for personal consumption, sports or fitness, weight loss, health supplements, food, or animal feed.

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3,5-Dinitrobenzoyl chloride Basic information

Product Name:	3,5-Dinitrobenzoyl chloride
Synonyms:	3,5-Dinitrobenzoicchloride;3,5-dinitrobenzoyl;3,5-dinitro-benzoylchlorid;DNBC;3,5-DINITROBENZOYL CHLORIDE;3,5-dinitrobenzoic acid chloride;3,4-DINITROBENZOYL CHLORIDE;3,5-DINITROBENZOYL CHLORIDE, FOR FLUORES CENCE
CAS:	99-33-2
MF:	C7H3ClN2O5
MW:	230.56
EINECS:	202-750-6
Product Categories:	API intermediates;Amino Group Labeling Reagents for HPLC;Hydroxyl Group Labeling Reagents for HPLC;Analytical Chemistry;HPLC Labeling Reagents;UV Detection (HPLC Labeling Reagents)
Mol File:	99-33-2.mol

3,5-Dinitrobenzoyl chloride Chemical Properties

Melting point	68-69 °C(lit.)
Boiling point	196 °C11 mm Hg(lit.)
density	1.8836 (rough estimate)
vapor density	7.6 (vs air)
refractive index	1.6290 (estimate)
Fp	196°C/12mm
storage temp.	2-8°C
form	Crystals or Crystalline Needles
color	Yellow to beige
Water Solubility	Slightly soluble in water.
Sensitive	Moisture Sensitive
Merck	14,3277
BRN	990249
Stability:	Stable. Incompatible with strong oxidizing agents, water, moisture, nitrates, combustible material. Refrigerate.
CAS DataBase Reference	99-33-2(CAS DataBase Reference)
NIST Chemistry Reference	Benzoyl chloride, 3,5-dinitro-(99-33-2)
EPA Substance Registry System	Benzoyl chloride, 3,5-dinitro- (99-33-2)

Safety Information

Hazard Codes	C
Risk Statements	34
Safety Statements	26-36/37/39-45-25
RIDADR	UN 3261 8/PG 2
WGK Germany	3
RTECS	DM6637000
F	21
Hazard Note	Corrosive
TSCA	Yes
HazardClass	8
PackingGroup	II
HS Code	29163900
HS Code	29400090

MSDS Information

Provider	Language
3,5-Dinitrobenzoyl chloride	English
SigmaAldrich	English
ACROS	English
ALFA	English

3,5-Dinitrobenzoyl chloride Usage And Synthesis

Chemical Properties	yellow-brown solid
Uses	3,5-dinitrobenzoyl chloride is an important intermediate for organic synthesis.
Uses	Used in photography. This aromatic compound is used by chemists to identify alcohol components in esters and in the fluorometric analysis of creatinine.
Purification Methods	Crystallise it from CCl4 or pet ether (b 40-60o). It reacts readily with H2O and should be kept in sealed ampoules. [Beilstein 9 IV 1350.]

3,5-Dinitrobenzoyl chloride Preparation Products And Raw materials

Raw materials	Thionyl chloride-->Carbon tetrachloride-->3,5-Dinitrobenzoic acid
Preparation Products	(+)-DISPARLURE-->Vitamin D2-->SAPERCONAZOLE-->3,5-DINITROBENZALDEHYDE-->(S)-(+)-N-(3,5-DINITROBENZOYL)-ALPHA-PHENYLGLYCINE

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